R-1,1'-联-2-萘酚合成路线 （共 56 条）
反应条件
C42H60N6O7 in toluene T=0°C; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 78, # 17 p. 8465 - 8484
反应条件
copper(l) iodide; methyllithium
参考文献
Chemistry - An Asian Journal, , vol. 6, # 2 p. 355 - 358
反应条件
1: FeCl3·6H2O 2: pyridine; 4-(N,N-dimethlyamino)pyridine / toluene; dichloromethane / 0 - 20 °C 3: Arthrobacter sp. lipase / dimethyl sulfoxide; aq. phosphate buffer / 36 h / 25 °C / pH 7 / |Resolution of racemate; |Enzymatic reaction View Scheme
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 101, p. 35 - 39
反应条件
in tetrahydrofuran T=-78 - 25°C; optical yield given as percent ee;
参考文献
Tetrahedron, , vol. 68, # 35 p. 7129 - 7132
反应条件
acetic acid 0.5 h; Heating;
参考文献
Cai, Jue Xiao; Zhou, Zheng Hong; Li, Kang Ying; Yeung, Chi Hung; Tang, Chu Chi
Phosphorus, Sulfur and Silicon and Related Elements, 2002 , vol. 177, # 1 p. 189 - 193
反应条件
in ethanol; hexane porcine pancreatic lipase, pH=7.4; Title compound not separated from byproducts;
参考文献
Miyano, Sotaro; Kawahara, Kan; Hashimoto Harukichi
Chemistry Letters, 1987 , p. 355 - 356
反应条件
(i) BBr3, CH2Cl2, (ii) H2O; Multistep reaction;
参考文献
Tetrahedron, , vol. 27, p. 5999 - 6009
反应条件
ph=5.5; enzymatic hydrolysis using fungi Absidia glauca or Rhizopus arrhizus;
参考文献
Wu, Shih-Hsiung; Zhang, Li-Qing; Chen, Ching-Shih; Girdaukas, Gary; Sih, C. J.
Tetrahedron Letters, 1985 , vol. 26, # 36 p. 4323 - 4326
反应条件
sodium hydroxide; tetra-(n-butyl)ammonium iodide in water T=20°C; 10 h;
参考文献
Hatano, Manabu; Horibe, Takahiro; Ishihara, Kazuaki
Journal of the American Chemical Society, 2010 , vol. 132, # 1 p. 56 - 57
反应条件
sodium hydroxide in water T=70 - 80°C;
参考文献
Gottarelli, Giovanni; Spada, Gian Piero
Journal of Organic Chemistry, 1991 , vol. 56, # 6 p. 2096 - 2098
