1,1,1,5,5,5-六甲基-3-[(三甲基硅烷基)氧基]-3-三硅氧烷基三(三甲基硅烷基)原硅酸盐合成路线 (共 21 条)
反应条件
lithium orthosilicate; acetic acid in N,N-dimethyl-formamide
参考文献
Kalmychkov, G. V.; Yarosh, N. K.; Mirskov, R. G.; Voronkov, M. G.; Rakhlin, V. I.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 10.2 p. 2282 - 2285,1881 - 1883
反应条件
scandium tris(trifluoromethanesulfonate) in acetonitrile T=20°C; 1 h;
参考文献
Hreczycho, Grzegorz; Pawluc, Piotr; Marciniec, Bogdan
New Journal of Chemistry, 2011 , vol. 35, # 12 p. 2743 - 2746
反应条件
bis-trimethylsilyl ether; olivine; water in butanone 1.) 5 min; 2.) 1 h;
参考文献
Kuroda, Kazuyuki; Koike, Tetsuhiro; Kato, Chuzo
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1981 , p. 1957 - 1960
参考文献
Mueller et al.
Journal fuer Praktische Chemie (Leipzig), 1959 , vol. <4>9, p. 63,67,70
反应条件
orthosilicic acid tetramethyl ester
参考文献
Voronkov,M.G. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1975 , vol. 24, p. 579 - 581
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1975 , vol. 24, p. 657 - 660
反应条件
bis-trimethylsilyl ether; rankinite 4 h; Ambient temperature;
参考文献
Calhoun, Harry P.; Masson, Charles R.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , # 8 p. 1282 - 1291
反应条件
tetrachlorosilane; sulfuric acid
参考文献
Mueller et al.
Journal fuer Praktische Chemie (Leipzig), 1959 , vol. <4>9, p. 63,67,70
反应条件
bis-trimethylsilyl ether; olivine; water; butan-1-ol 1.) 5 min; 2.) 1 h;
参考文献
Kuroda, Kazuyuki; Koike, Tetsuhiro; Kato, Chuzo
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1981 , p. 1957 - 1960
反应条件
bis-trimethylsilyl ether; olivine; water 1.) 5 min; 2.) 1 h; Further byproducts given;
参考文献
Kuroda, Kazuyuki; Koike, Tetsuhiro; Kato, Chuzo
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1981 , p. 1957 - 1960
反应条件
bis-trimethylsilyl ether; olivine; water 1.) 5 min; 2.) 1 h; Further byproducts given;
参考文献
Kuroda, Kazuyuki; Koike, Tetsuhiro; Kato, Chuzo
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1981 , p. 1957 - 1960