N,N-双(2-羟基苯)乙烯二胺合成路线 (共 8 条)
反应条件
sodium tetrahydroborate in dichloromethane
参考文献
Voronova, Krisztina; Purgel, Mihaly; Udvardy, Antal; Benyei, Attila C.; Katho, Agnes; Joo, Ferenc
Organometallics, 2013 , vol. 32, # 15 p. 4391 - 4401
反应条件
1: 95 percent / methanol 2: 61 percent / NaBH4; KOH; methanol / CH2Cl2 / 0 °C / pH 6 View Scheme
参考文献
Sharma, Vibha; Khan
European Journal of Medicinal Chemistry, 2001 , vol. 36, # 7-8 p. 651 - 658
反应条件
1: With hydrogenchloride in 1,4-dioxane 2: With ammonium hydroxide in methanol
参考文献
Rivera, Augusto; Quevedo, Rodolfo; Navarro, Miguel A.; Maldonado, Mauricio
Synthetic Communications, 2004 , vol. 34, # 13 p. 2479 - 2485
反应条件
1: in isopropyl alcohol Acidic conditions; 2: With sodium tetrahydroborate in ethanol
参考文献
Carril, Monica; Altmann, Philipp; Drees, Markus; Bonrath, Werner; Netscher, Thomas; Schuetz, Jan; Kuehn, Fritz E.
Journal of Catalysis, 2011 , vol. 283, # 1 p. 55 - 67
反应条件
1: methanol 2: sodium tetrahydroborate / dichloromethane View Scheme
参考文献
Kalyanam, N; Parthasarathy, P C; Ananthan, L; Manjunatha, S G; Likhate, M A
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 4 p. 243 - 247
反应条件
1: 97 percent 2: 22 percent / 30percent H2O2, sodium hydroxide / ethanol; H2O / 3 h / 5 - 10 °C 3: 1.) Fe(III) salt, 2.) 8-hydroxyquinoline / 1.) Fe(III) salt, neutral or alkaline pH, 3-4 h, RT; 2.) HCl, pH = 5.0, 8-hydroxyquinoline/ethanol, 50 deg C View Scheme
参考文献
Martell, Arthur E.; Motekaitis, Ramunas J.; Clarke, Eric T.; Harrison, J.J.
Canadian Journal of Chemistry, 1986 , vol. 64, p. 449 - 456
反应条件
in benzene
0.133333 h; Heating;
参考文献
Billman,J.H.; Dorman,L.C.
J. Med. Chem., 1963 , vol. 6, p. 701 - 705
反应条件
toluene-4-sulfonic acid in butan-1-ol
0.666667 h; Reflux;
参考文献
Tolpygin; Shepelenko; Revinskii; Tsukanov; Dubonosov; Bren; Minkin
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 8 p. 1181 - 1184