3-苯基-2-丙烯酸-2-丙烯基酯合成路线 (共 17 条)
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; 1,3-bis(2,4,6-trimethylphenyl)imidazolinium chloride in tetrahydrofuran T=20°C; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Tetrahedron, , vol. 68, # 32 p. 6498 - 6503
反应条件
1: allyl alcohol With 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-dimethyl-1H-1,2,4-triazol-4-ium iodide in tetrahydrofuran 0.0833333 h; Inert atmosphere; 2: (E)-cinnamaldehyde With 3,3',5,5'-tetra-tert-butyl-4,4'-diphenoquinone in tetrahydrofuran T=20°C; 2 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 132, p. 1190 - 1191
反应条件
silica gel-immobilized perchloric acid T=80°C; Fischer esterification; 5 h; Inert atmosphereNeat (no solvent);
参考文献
Journal of Organic Chemistry, , vol. 74, # 16 p. 5967 - 5974
反应条件
potassium fluoride; tetra(n-butyl)ammonium hydrogensulfate in tetrahydrofuran T=20°C; 72 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 6 p. 973 - 984
反应条件
in tetrahydrofuran T=60°C; 16 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 18 p. 5897 - 5905
反应条件
in acetonitrile T=120°C; 0.025 h; Microwave irradiation;
参考文献
Journal of Organic Chemistry, , vol. 74, # 13 p. 4753 - 4762
反应条件
4-(N,N-dimethlyamino)pyridine in tetrahydrofuran 22 h;
参考文献
Synthesis, , # 10 p. 1063 - 1066
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile 1 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 36, # 1 p. 113 - 114
反应条件
in toluene T=90°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 43, # 5 p. 907 - 909
反应条件
1: allyl diphenylphosphonoacetate With N-benzyl-trimethylammonium hydroxide in methanol T=-78°C; Elimination; 0.166667 h; 2: benzaldehyde in tetrahydrofuran; methanol T=-78°C; Condensation; Horner-Wadsworth-Emmons reaction; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 64, # 22 p. 8406 - 8408