5-(2,5-二氯苯基)-2-糠酸合成路线 (共 5 条)
反应条件
1: 1,4-Dichloro-2-aminobenzene With hydrogenchloride; sodium nitrite 2: furan-2-carboxylic acid With CuCl2*2H2O in water; acetone T=0 - 30°C;
参考文献
Gorak; Obushak; Matiichuk; Lytvyn
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 4 p. 541 - 550
反应条件
1: Na2CO3 / Pd(PPh3)4 / 1,2-dimethoxy-ethane / 100 °C 2: aq. LiOH / tetrahydrofuran View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 17, # 12 p. 3258 - 3261
反应条件
1: Na2CO3 / Pd(PPh3)4 / 1,2-dimethoxy-ethane / 100 °C 2: aq. LiOH / tetrahydrofuran View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 17, # 12 p. 3258 - 3261
反应条件
lithium hydroxide in tetrahydrofuran
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 17, # 12 p. 3258 - 3261
反应条件
thionyl chloride in benzene
Reflux;
参考文献
Gorak; Obushak; Matiichuk; Lytvyn
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 4 p. 541 - 550