丙酸(1R,2S)-2-[N-苄基-N-(均三甲苯基磺酰)氨基]-1-苯基丙酯合成路线 （共 5 条）
反应条件
pyridine in dichloromethane T=0 - 20°C; Acylation;
参考文献
Inoue, Tadashi; Liu, Ji-Feng; Buske, Dana C.; Abiko, Atsushi
Journal of Organic Chemistry, 2002 , vol. 67, # 15 p. 5250 - 5256
反应条件
1: 100 percent / triethylamine / CH2Cl2 / 2 h / 0 - 20 °C 2: 95 percent / potassium carbonate / acetonitrile / 7 h / Heating 3: 100 percent / pyridine / CH2Cl2 / 13 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 67, # 15 p. 5250 - 5256
反应条件
1: 95 percent / potassium carbonate / acetonitrile / 7 h / Heating 2: 100 percent / pyridine / CH2Cl2 / 13 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 67, # 15 p. 5250 - 5256
反应条件
1: 100 percent / triethylamine / CH2Cl2 2: 95 percent / K2CO3 / acetonitrile / 7 h / Heating 3: 100 percent / pyridine / CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 119, # 10 p. 2586 - 2587
反应条件
1.1: dicyclohexylboron triflate; triethylamine / CH2Cl2; hexane / 2 h / -78 °C 1.2: 98 percent / CH2Cl2; hexane / 2 h / -78 - 20 °C 2.1: 4.20 g / lithium aluminum hydride / tetrahydrofuran / 1 h / 20 °C View Scheme
参考文献
Inoue, Tadashi; Liu, Ji-Feng; Buske, Dana C.; Abiko, Atsushi
Journal of Organic Chemistry, 2002 , vol. 67, # 15 p. 5250 - 5256
