187737-37-7合成路线 （共 2341 条）
参考文献
Kryuchkova,V.G.; Zavgorodnii,S.V.
J. Gen. Chem. USSR (Engl. Transl.), 1961 , vol. 31, # 2 p. 374 - 377,338 - 340
反应条件
in neat (no solvent) react. Ge, HCl and alkene in a fix-bed flow reactor at 400°C; detected by GC-MS;
参考文献
Okamoto, Masaki; Asano, Takuya; Suzuki, Eiichi
Dalton Transactions, 2004 , # 15 p. 2372 - 2376
反应条件
hydrogen fluoride; chlorine T=236 - 291°C; P=2585.81 Torr; Further byproducts.;
参考文献
Belter, Randolph K.
Journal of Fluorine Chemistry, 2006 , vol. 127, # 12 p. 1611 - 1615
参考文献
Alder,K.; von Brachel,H.
Justus Liebigs Annalen der Chemie, 1962 , vol. 651, p. 141 - 153
反应条件
1,3-dibromo-5,5-dimethyl-hydantoin; hydrogen fluoride in pyridine T=-78°C; 0.166667 h;
参考文献
Chi, Dae Yoon; Kiesewetter, Dale O.; Katzenellenbogen, John A.
Journal of Fluorine Chemistry, 1986 , vol. 31, p. 99 - 114
反应条件
sulfur(IV) fluoride; hydrogen fluoride; bromine T=20°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Kunshenko, B. V.; Mokhamed, Nagib Mukhtar; Omarov, V. O.; Muratov, N. N.; Yagupol'skii, L. M.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 4.1 p. 511 - 518
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 4 p. 672 - 680
反应条件
N-bromosuccinmide; triethylamine tris(hydrogen fluoride) in dichloromethane 1.) 0 deg C, 15 min, 2.) r.t., 5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kroeger, Stefan; Haufe, Guenter
Liebigs Annalen/Recueil, 1997 , # 6 p. 1201 - 1206
参考文献
Danno,S. et al.
Tetrahedron, 1969 , vol. 25, p. 4809 - 4813
反应条件
in n-heptane High Pressure; (Ar); to a soln. of Al-compound added propene (13 bar pressure) under stirring at 100°C for 40 h; distd. in vacuo; elem. anal.;
参考文献
Martin, Heinz; Bretinger, Helmut
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1985 , vol. 40, # 2 p. 182 - 186
反应条件
in n-heptane byproducts: (C3H7)2AlCl; High Pressure; (Ar); to a soln. of Al-compound and Al added propene (19.5 bar pressure) under stirring at 100°C for 24 h; distd. in vacuo; elem. anal.;
参考文献
Martin, Heinz; Bretinger, Helmut
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1985 , vol. 40, # 2 p. 182 - 186
