2,6-二甲基辛-7-烯-4-酮合成路线 (共 15 条)
反应条件
aluminum oxide; zinc(II) chloride T=-10°C; Alkylation; 1.5 h;
参考文献
Kad; Singh, Vasundhara; Khurana, Anupam; Chaudhary, Sangeeta; Singh, Jasvinder
Synthetic Communications, 1999 , vol. 29, # 19 p. 3439 - 3442
反应条件
1: DBU / CH2Cl2 / 1 h / 40 °C 2: 64 percent / ZnCl2 doped on acidic alumina / 1.5 h / -10 °C View Scheme
参考文献
Synthetic Communications, , vol. 29, # 19 p. 3439 - 3442
反应条件
1: SOCl2 2: (i) Mg, (ii) CdCl2, (iii) /BRN= 1921936/ View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 41, # 11 p. 752 - 754
反应条件
1: AgNO3, aq. NaOH 2: SOCl2 3: (i) Mg, (ii) CdCl2, (iii) /BRN= 1921936/ View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 41, # 11 p. 752 - 754
反应条件
1: (i) , (ii) (acid hydrolysis) 2: (i) , (ii) Py*HClCrO3 View Scheme
参考文献
Tetrahedron Letters, , p. 1379 - 1380
反应条件
(i) LDA, Et2O, THF, (ii) /BRN= 1769652/, (iii) (heating); Multistep reaction;
参考文献
Tetrahedron Letters, , p. 3713 - 3716
反应条件
(i) , (ii) Py*HClCrO3; Multistep reaction;
参考文献
Tetrahedron Letters, , p. 1379 - 1380
反应条件
(i) Al(OiPr)3, Al(OsBu)3, (ii) (pyrolysis); Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 367 - 369
反应条件
(i) Mg, (ii) CdCl2, (iii) /BRN= 1921936/; Multistep reaction;
参考文献
Journal of the Indian Chemical Society, , vol. 41, # 11 p. 752 - 754
反应条件
T=0°C; dextrorotatory form;
参考文献
Jones; Smith
Journal of the Chemical Society, 1925 , vol. 127, p. 2535