n-butyllithium; potassium tert-butylate in tetrahydrofuran; hexane
T=-105°C;
参考文献
Verbeek, Jacob; George, Albert V. E.; Jong, Robertus L. P. de; Brandsma, Lambert
Journal of the Chemical Society, Chemical Communications, 1984 , # 4 p. 257 - 258
Dunne, Simon J.; Summers, Lindsay A.; Nagy-Felsobuky, Ellak I. von
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 72, # 1-4 p. 103 - 120
1: With n-butyllithium; 2-(dimethylamino)-ethanol in tetrahydrofuran; toluene
T=-95°C; 4 h;
2: With carbon tetrabromide in tetrahydrofuran; toluene
T=-95°C; 15 h;
titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate in dichloromethane; water; toluene
T=-50°C; 72 h; Yield given. Title compound not separated from byproducts;
参考文献
Boussad, N.; Trefouel, T.; Dupas, G.; Bourguignon, J.; Queguiner, G.
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 66, # 1.4 p. 127 - 138
Boussad, N.; Trefouel, T.; Dupas, G.; Bourguignon, J.; Queguiner, G.
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 66, # 1.4 p. 127 - 138
