反应条件
ethanol in 1,4-dioxane
byproducts: Cl2(O)PN(C2H5)P(O)Cl2, POCl2(OC2H5), (C2H5O)Cl2PNP(O)Cl2; addn. of EtOH in dioxane to suspn. of (Cl3PNPCl3)PCl6 in dioxane (molar ratio 2:1) at ambient temp. during 1 h; not isolated; (31)P-NMR spectroscopic monitoring;
参考文献
Heubel, Joseph; Hammoutou, Yahia; Jaeger, Roger De
Phosphorus, Sulfur, and Silicon and the Related Elements, 1991 , vol. 63, p. 19 - 32
