188290-36-0合成路线 （共 917 条）
反应条件
n-butyllithium
1.) hexane/THF, 0 deg C -> room temperature, 2.) hexane/THF, reflux, 1 h; Yield given. Multistep reaction;
参考文献
Barton, Thomas J.; Hussmann, Gregory P.
Journal of Organic Chemistry, 1985 , vol. 50, # 26 p. 5881 - 5882
参考文献
Coonradt et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 163
参考文献
Coonradt et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 163
参考文献
Wynberg; Bantjes
Journal of Organic Chemistry, 1959 , vol. 24, p. 1421
反应条件
in thiophene
was heated at 70°C for 2h; was filtered; filtrate was concentrated under reduced pressure; was diluted with hexane; GLC;
参考文献
Fuchita, Yoshio; Hiraki, Katsuma; Kamogawa, Yasuko; Suenaga, Miho; Tohgoh, Kazutaka; Fujiwara, Yuzo
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 4 p. 1081 - 1085
参考文献
Wynberg; Bantjes
Journal of Organic Chemistry, 1959 , vol. 24, p. 1421
反应条件
T=876.84 - 926.84°C; IR laser powering; Product distribution; Further Variations:Reagents;
参考文献
Hore, Nathan R.; Russell, Douglas K.
New Journal of Chemistry, 2004 , vol. 28, # 5 p. 606 - 613
反应条件
potassium tert-butylate in dimethyl sulfoxide
T=20°C; 5 h; Schlenk techniqueInert atmosphereIrradiation; TimeConcentration; Overall yield = 59 percent;
参考文献
Buden, Maria E.; Guastavino, Javier F.; Rossi, Roberto A.
Organic Letters, 2013 , vol. 15, # 6 p. 1174 - 1177
反应条件
potassium acetate; palladium diacetate in N,N-dimethyl acetamide
T=130°C; 4 h;
参考文献
ENI S.p.A.; SCHIMPERNA, Giuliana; BIANCHI, Gabriele
Patent: WO2013/21315 A1, 2013 ;
Location in patent: Page/Page column 26-27 ;
反应条件
kieselguhr; phosphoric acid
T=270°C; P=14710.2 Torr;
参考文献
Appleby et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 1552
