188290-36-0合成路线 （共 917 条）
参考文献
Novak et al.
Collection of Czechoslovak Chemical Communications, 1957 , vol. 22, p. 1836,1845
反应条件
copper(l) chloride in diethyl ether
1.) reflux, 3 h, 2.) RT, 1 h; Yields of byproduct given;
参考文献
Golz, Thomas; Hammes, Susann; Klaerner, Frank-Gerrit
Chemische Berichte, 1993 , vol. 126, # 2 p. 485 - 498
反应条件
copper(l) chloride
1a.) ether, reflux, 1b.) RT, 1 h, 2a.) ether, reflux, 2b.) RT, 12 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Golz, Thomas; Hammes, Susann; Klaerner, Frank-Gerrit
Chemische Berichte, 1993 , vol. 126, # 2 p. 485 - 498
反应条件
1.) glow discharge, 2.) -196 deg C -> -80 deg C; Further byproducts given. Title compound not separated from byproducts;
参考文献
Skramstad, Jan; Chaudhry, Mohammed Shoaib; Garvang, Arne
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1984 , vol. 38, # 6 p. 509 - 512
反应条件
1.) glow discharge, 2.) -196 deg C -> -80 deg C; Further byproducts given. Title compound not separated from byproducts;
参考文献
Skramstad, Jan; Chaudhry, Mohammed Shoaib; Garvang, Arne
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1984 , vol. 38, # 6 p. 509 - 512
反应条件
phosphoric acid
T=288°C; P=14710.2 Torr;
参考文献
Appleby et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 1552
反应条件
oxygen; trimethylamine
T=37.5°C; P=5 - 760 Torr; Irradiation; Yield given. Title compound not separated from byproducts;
参考文献
Laguzzi, Giuseppe; Speranza, Maurizio
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 857 - 866
反应条件
aluminium trichloride in 1,2-dichloro-ethane
-30 deg C, 1 h, RT, 2 d;
参考文献
Belen'kii, L. I.; Yakubov, A. P.
Tetrahedron, 1986 , vol. 42, # 2 p. 759 - 762
反应条件
T=288°C; P=15813.4 Torr;
参考文献
Appleby et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 1552
反应条件
aluminium trichloride; water
1.) CH2Cl2, -70 deg C, 1 h; rt, 2 days; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Belen'kii, L. I.; Yakubov, A. P.
Tetrahedron, 1984 , vol. 40, # 13 p. 2471 - 2477
