二甲氨基亚甲基二磷酸四乙酯合成路线 （共 18 条）
反应条件
hydrogenchloride; sodium hydride 1.) 80 deg C, 3 h, 2.) heated on water bath; Yield given. Multistep reaction;
参考文献
Majeed, Amera J.; Sainsbury, Malcolm; Hall, Stephen A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 4 p. 833 - 837
反应条件
1: N,N-dimethyl-formamide With oxalyl dichloride in diethyl ether
T=20°C; 1 h; Cooling;
2: triethyl phosphite in diethyl ether
1 h;
参考文献
O'Boyle, Niamh M.; Greene, Lisa M.; Bergin, Orla; Fichet, Jean-Baptiste; McCabe, Thomas; Lloyd, David G.; Zisterer, Daniela M.; Meegan, Mary J.
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 7 p. 2306 - 2325
反应条件
zinc(II) chloride
T=130°C;
参考文献
Prishchenko, Andrey A.; Livantsov, Mikhail V.; Novikova, Olga P.; Livantsova, Ludmila I.; Petrosyan, Valery S.
Heteroatom Chemistry, 2009 , vol. 20, # 6 p. 319 - 324
反应条件
hydrogenchloride; ethanethiol in acetic acid
Ambient temperature;
参考文献
Gross, Hans; Keitel, Iris; Costisella, Burkhard; Mikolajczyk, Marian; Midura, Wanda
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 257 - 262
反应条件
T=110 - 130°C; 2.5 h;
参考文献
Prishchenko, A. A.; Livantsov, M. V.; Petrosyan, V. S.
Russian Journal of General Chemistry, 1993 , vol. 63, # 8.2. p. 1326 - 1327
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 8 p. 1902 - 1903
反应条件
in dichloromethane
T=-15 - 170°C;
参考文献
Riesel,L. et al.
Journal fuer Praktische Chemie (Leipzig), 1978 , vol. 320, p. 389 - 394
参考文献
Gross,H. et al.
Journal fuer Praktische Chemie (Leipzig), 1969 , vol. 311, p. 577 - 585
反应条件
in N,N-dimethyl-formamide
参考文献
Costisella,B.; Gross,H.
Journal fuer Praktische Chemie (Leipzig), 1979 , vol. 321, p. 361 - 369
参考文献
Gross,H. et al.
Journal fuer Praktische Chemie (Leipzig), 1969 , vol. 311, p. 577 - 585
参考文献
Gross,H. et al.
Journal fuer Praktische Chemie (Leipzig), 1969 , vol. 311, p. 577 - 585
