N,N-二乙基-3-苯基丙酰胺合成路线 （共 30 条）
反应条件
samarium diiodide; water; triethylamine in tetrahydrofuran T=20°C; Inert atmosphere;
参考文献
Szostak, Michal; Sautier, Brice; Spain, Malcolm; Procter, David J.
Organic Letters, 2014 , vol. 16, # 4 p. 1092 - 1095
反应条件
samarium diiodide; water; triethylamine in tetrahydrofuran T=23°C; 18 h; Inert atmosphereSchlenk technique; Kinetics; chemoselective reaction;
参考文献
Szostak, Michal; Spain, Malcolm; Eberhart, Andrew J.; Procter, David J.
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2268 - 2271
反应条件
Schwartz's reagent in tetrahydrofuran T=20°C; 0.25 h;
参考文献
Journal of the American Chemical Society, , vol. 122, # 48 p. 11995 - 11996
Journal of the American Chemical Society, , vol. 129, # 11 p. 3408 - 3419
参考文献
Maxim
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1926 , vol. 182, p. 1395
Annales de Chimie (Cachan, France), 1928 , vol. <10> 9, p. 69,76
参考文献
Maxim
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1926 , vol. 182, p. 1395
Annales de Chimie (Cachan, France), 1928 , vol. <10> 9, p. 69,76
反应条件
pyridine; trifluoromethylsulfonic anhydride 1.) CH2Cl2, -40 to 0 deg C, 2 h; 0 deg C, 2 h, 2.) r.t., 4 h; Yield given. Multistep reaction;
参考文献
Charette, Andre B.; Chua, Peter
Synlett, 1998 , # 2 p. 163 - 165
参考文献
Maxim
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1926 , vol. 182, p. 1395
Annales de Chimie (Cachan, France), 1928 , vol. <10> 9, p. 69,76
反应条件
cerium(III) chloride; methyllithium in tetrahydrofuran T=-78°C; 0.25 h; Yield given. Yields of byproduct given;
参考文献
Kurosu, Michio; Kishi, Yoshito
Tetrahedron Letters, 1998 , vol. 39, # 27 p. 4793 - 4796
反应条件
samarium diiodide; water; triethylamine in tetrahydrofuran T=20°C; Inert atmosphere;
参考文献
Szostak, Michal; Sautier, Brice; Spain, Malcolm; Procter, David J.
Organic Letters, 2014 , vol. 16, # 4 p. 1092 - 1095
反应条件
hydrogen in ethanol; water
T=25°C; P=760.051 Torr; 12 h; chemoselective reaction;
参考文献
Morimoto, Naoki; Yamamoto, Shun-Ichi; Takeuchi, Yasuo; Nishina, Yuta
RSC Advances, 2013 , vol. 3, # 36 p. 15608 - 15612
