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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
188980-05-4
合成路线
（共 12 条）
207727-09-1
→
反应条件
188980-05-4
反应条件
water; sodium chloride in dimethyl sulfoxide T=150°C; 18 h;
参考文献
COUNCIL OF SCIENTIFIC AND INDUSTRIAL RESEARCH
Patent: US2007/191606 A1, 2007 ;
Location in patent: Page/Page column 5 ;
33965-97-8
→
反应条件
188980-05-4
反应条件
1: With oxygen; ozone; acetic acid in dichloromethane T=-4 - -2°C; 2: With sodium tris(acetoxy)borohydride in dichloromethane T=20°C; 3 h;
参考文献
Ishmuratov; Yakovleva; Kharisov; Botsman; Izibairov; Mannapov; Tolstikov
Chemistry of Natural Compounds, 2001 , vol. 37, # 2 p. 190 - 192
5602-17-5
→
反应条件
188980-05-4
反应条件
1: With oxygen; ozone; acetic acid in dichloromethane T=-4 - -2°C; 2: With sodium tris(acetoxy)borohydride in dichloromethane T=20°C;
参考文献
Ishmuratov; Yakovleva; Kharisov; Botsman; Izibairov; Mannapov; Tolstikov
Chemistry of Natural Compounds, 2001 , vol. 37, # 2 p. 190 - 192
112-47-0
1,10-癸二醇
+
67-64-1
丙酮
→
反应条件
188980-05-4
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; triphenylphosphine; potassium hydroxide in toluene T=80°C; 0.5 h; Inert atmosphere;
参考文献
Iuchi, Yosuke; Hyotanishi, Megumi; Miller, Brittany E.; Maeda, Kensaku; Obora, Yasushi; Ishii, Yasutaka
Journal of Organic Chemistry, 2010 , vol. 75, # 5 p. 1803 - 1806
73125-64-1
→
反应条件
188980-05-4
反应条件
sodium tris(acetoxy)borohydride in benzene 2.5 h;
参考文献
Odinokov, V. N.; Ishmuratov, G. Yu.; Ladenkova, I. M.; Tolstikov, G. A.
Chemistry of Natural Compounds, 1992 , vol. 28, # 2 p. 235 - 236
Khimiya Prirodnykh Soedinenii, 1992 , # 2 p. 270 - 272
947-05-7
氧杂环十三烷-2-酮
+
917-54-4
甲基锂
→
反应条件
188980-05-4
反应条件
1: LLON With methyllithium; O,N-dimethyl-hydroxylamine hydrochloride in tetrahydrofuran T=0 - 20°C; 2: methyllithium in tetrahydrofuran T=0 - 20°C;
参考文献
Muller, Thierry; Coowar, Djalil; Hanbali, Mazen; Heuschling, Paul; Luu, Bang
Tetrahedron, 2006 , vol. 62, # 51 p. 12025 - 12040
830-13-7
环十二酮
→
反应条件
188980-05-4
反应条件
1.1: 85 percent / m-chloroperbenzoic acid; acetic acid / CH2Cl2 / 24 h / Heating 2.1: N,O-dimethylhydroxylamine hydrochloride; methyllithium / tetrahydrofuran / 0 - 20 °C 2.2: tetrahydrofuran / 0 - 20 °C View Scheme
参考文献
Muller, Thierry; Coowar, Djalil; Hanbali, Mazen; Heuschling, Paul; Luu, Bang
Tetrahedron, 2006 , vol. 62, # 51 p. 12025 - 12040
141-97-9
乙酰乙酸乙酯
+
4101-68-2
1,10-二溴癸烷
→
反应条件
188980-05-4
反应条件
sodium methylate; potassium iodide T=100°C; behandeln des Reaktionsprodukts mit aethanol.Kalilauge;
参考文献
Stoll
Helvetica Chimica Acta, 1951 , vol. 34, p. 1818
7766-50-9
溴代十一碳烯
→
反应条件
188980-05-4
反应条件
1.1: 89 percent / Na; EtOH / 18 h / Heating 2.1: 81 percent / LiI / dimethylformamide / 12 h / Heating 3.1: ozone; oxygen; acetic acid / CH2Cl2 / -4 - -2 °C 3.2: 98 percent / sodium triacetoxyborohydride / CH2Cl2 / 3 h / 20 °C View Scheme
参考文献
Ishmuratov; Yakovleva; Kharisov; Botsman; Izibairov; Mannapov; Tolstikov
Chemistry of Natural Compounds, 2001 , vol. 37, # 2 p. 190 - 192
157373-99-4
→
反应条件
188980-05-4
反应条件
1.1: 81 percent / LiI / dimethylformamide / 12 h / Heating 2.1: ozone; oxygen; acetic acid / CH2Cl2 / -4 - -2 °C 2.2: 98 percent / sodium triacetoxyborohydride / CH2Cl2 / 3 h / 20 °C View Scheme
参考文献
Ishmuratov; Yakovleva; Kharisov; Botsman; Izibairov; Mannapov; Tolstikov
Chemistry of Natural Compounds, 2001 , vol. 37, # 2 p. 190 - 192
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