N,N-二甲基-2-苯基乙酰胺合成路线 (共 47 条)
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride
参考文献
Ishibashi, Hiroyuki; Nakamura, Nobuyuki; Ito, Katsuhiro; Kitayama, Shinji; Ikeda, Masazumi
Heterocycles, 1990 , vol. 31, # 10 p. 1781 - 1784
反应条件
potassium hydroxide; bis(o-nitrophenyl)phenylphosphonate; 4 A molecular sieve; tetrabutylammomium bromide; triethylamine
1.) THF/water, 1 h, 2.) THF, RT, 3 h; Yield given. Multistep reaction;
参考文献
Watanabe, Yutaka; Mukaiyama, Teruaki
Chemistry Letters, 1981 , p. 285 - 288
参考文献
Skrowaczewska; Mastalerz
Roczniki Chemii, 1957 , vol. 31, p. 531,535
Chem.Abstr., 1958 , p. 2798
参考文献
Morel,G. et al.
Bulletin de la Societe Chimique de France, 1975 , p. 1865 - 1870
参考文献
Rossi, Roberto A.; Alonso, Ruben A.
Journal of Organic Chemistry, 1980 , vol. 45, # 7 p. 1239 - 1241
反应条件
potassium hydroxide; bis(o-nitrophenyl)phenylphosphonate; 4 A molecular sieve; tetrabutylammomium bromide
other amines; multistep reaction;
参考文献
Watanabe, Yutaka; Mukaiyama, Teruaki
Chemistry Letters, 1981 , p. 285 - 288
反应条件
in acetonitrile
0.0833333 h; Inert atmosphereIrradiation;
参考文献
Allen, Annette D.; Andraos, John; Tidwell, Thomas T.; Vukovic, Sinisa
Journal of Organic Chemistry, 2014 , vol. 79, # 2 p. 679 - 685
反应条件
(i) <Me3O>BF4, (ii) aq. Na2CO3; Multistep reaction;
参考文献
Mukherjee,R.
Journal of the Chemical Society [Section] D: Chemical Communications, 1971 , p. 1113 - 1114
参考文献
Farbenfabr. Bayer
Patent: DE875807 , 1951 ;
反应条件
potassium hydroxide; bis(o-nitrophenyl)phenylphosphonate; 4 A molecular sieve; tetrabutylammomium bromide; triethylamine
reaction also with carboxylic esters; multistep reaction;
参考文献
Watanabe, Yutaka; Mukaiyama, Teruaki
Chemistry Letters, 1981 , p. 285 - 288