1: (E)-4-phenyl-3-buten-2-one With [{(Ph3P)CuH}6]; hydrogen; (dimethyl)(phenyl)phosphine in tert-butyl alcohol; benzene T=20°C; Hydrogenation; P=25857.4 Torr; 18 h; 2: acetic anhydride With pyridine in tert-butyl alcohol; benzene T=0 - 20°C; Acetylation; Title compound not separated from byproducts;
参考文献
Chen, Jian-Xin; Daeuble, John F.; Brestensky, Donna M.; Stryker, Jeffrey M.
Tetrahedron, 2000 , vol. 56, # 15 p. 2153 - 2166