二-μ-氯双[2-[(二甲氨基)甲基]苯基-C,N]二钯(Ⅱ)合成路线 (共 7 条)
反应条件
in methanol addn. of NaCl to suspn. of PdCl2, stirring (1 h), dropwise addn. of soln. of aminoborinic acid ester (pptn. over 3 h); filtration;
参考文献
Vogels, Christopher M.; Wellwood, Heather L.; Biradha, Kumar; Zaworotko, Michael J.; Westcott, Stephen A.
Canadian Journal of Chemistry, 1999 , vol. 77, # 7 p. 1196 - 1207
反应条件
1: diethyl ether; water; hexane 2: dichloromethane 3: methanol View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 77, # 7 p. 1196 - 1207
反应条件
1: dichloromethane 2: methanol View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 77, # 7 p. 1196 - 1207
反应条件
1: dichloromethane 2: dichloromethane View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 77, # 7 p. 1196 - 1207
反应条件
1: diethyl ether; water; hexane 2: dichloromethane 3: dichloromethane View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 77, # 7 p. 1196 - 1207
反应条件
in methanol addn. of NaCl to suspn. of PdCl2, stirring (1 h), dropwise addn. of soln. of aminoborinic acid (pptn. over 1 h); filtration, washing (water);
参考文献
Canadian Journal of Chemistry, , vol. 77, # 7 p. 1196 - 1207
反应条件
in dichloromethane dropwise addn. of soln. of aminoborinic acid ester to soln. of Pd complex (stirring, 6 h); solvent removal, not sepd., reaction followed by NMR spectroscopy;
参考文献
Canadian Journal of Chemistry, , vol. 77, # 7 p. 1196 - 1207