甲基10-氧代十一烷酸酯合成路线 （共 18 条）
反应条件
[Co(PPh3)3Cl]
6 h; Ambient temperature; Yield given. Further byproducts given;
参考文献
Momose, Den-ichi; Yamada, Yasuji
Tetrahedron Letters, 1983 , vol. 24, # 26 p. 2669 - 2672
反应条件
methyllithium
1) ether, 20 deg C; 2) ether; Yield given. Multistep reaction;
参考文献
Marko, Istvan E.; Southern, J. Mike
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3368 - 3370
反应条件
titanium(III) chloride; sulfuric acid; dihydrogen peroxide
1.) 2 h, room temp., 2.) 30 min,; Yield given. Multistep reaction;
参考文献
Citterio; Vismara
Synthesis, 1980 , vol. No. 9, p. 751 - 753
反应条件
palladium on activated charcoal
Hydrogenation;
参考文献
Iritani et al.
Yakugaku Zasshi, 1957 , vol. 77, p. 1036
Chem.Abstr., 1958 , p. 2743
反应条件
Multistep reaction. Title compound not separated from byproducts;
参考文献
Odinokov, V. N.; Botsman, L. P.; Ishmuratov, G. Yu.; Tolstikov, G. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 453 - 463
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 3 p. 524 - 537
反应条件
[Co(PPh3)3Cl]
6 h; Ambient temperaturedepending on presence of additive; Product distribution;
参考文献
Momose, Den-ichi; Yamada, Yasuji
Tetrahedron Letters, 1983 , vol. 24, # 26 p. 2669 - 2672
反应条件
1: 72 percent / n-BuLi / tetrahydrofuran / -20 °C
2: 100 percent / hydrogen / Pd/C / ethanol / 20 °C
3: 95 percent / LAH / diethyl ether / Heating
View Scheme
参考文献
Sharma, Anubha; Gamre, Sunita; Chattopadhyay, Subrata
Tetrahedron Letters, 2007 , vol. 48, # 21 p. 3705 - 3707
反应条件
1: 72 percent / n-BuLi / tetrahydrofuran / -20 °C
2: 100 percent / hydrogen / Pd/C / ethanol / 20 °C
View Scheme
参考文献
Sharma, Anubha; Gamre, Sunita; Chattopadhyay, Subrata
Tetrahedron Letters, 2007 , vol. 48, # 21 p. 3705 - 3707
