3-甲基-4-苯基-3-丁烯-2-酮合成路线 (共 16 条)
反应条件
ruthenium trichloride T=120°C; Condensation; 16 h; Heating;
参考文献
Iranpoor, Nasser; Kazemi, Foad
Tetrahedron, 1998 , vol. 54, # 32 p. 9475 - 9480
反应条件
PdBr2(CH3CN)2; oxygen; caesium carbonate; (+)-sparteine surrogate in chloroform T=20°C; 35 h; Molecular sieve; optical yield given as percent ee;
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 34 p. 6367 - 6370
反应条件
palladium dichloro (η-2,5-norbornadiene); oxygen; caesium carbonate; (-)-sparteine in chloroform T=23°C; 48 h; Molecular sieve; optical yield given as percent eeenantiospecific reaction;
参考文献
Journal of the American Chemical Society, , vol. 130, # 47 p. 15957 - 15966
反应条件
PEG-400; potassium carbonate T=90°C; aldol condensation; 2.5 h;
参考文献
Cao, Yu-Qing; Dai, Zhi; Zhang, Rui; Chen, Bao-Hua
Synthetic Communications, 2005 , vol. 35, # 8 p. 1045 - 1049
反应条件
[oxorhenium(V)trichloride(SMe2)(OPPh3)] in 1,4-dioxane T=20°C; Meyer-Schuster rearrangement; 3 h;
参考文献
Chemistry - A European Journal, , vol. 16, # 31 p. 9555 - 9562
反应条件
chromium(VI) oxide T=0 - 56°C; 10 h;
参考文献
Chinese Journal of Chemistry, , vol. 29, # 10 p. 2086 - 2090
反应条件
oxalic acid; silica gel 1.) THF, -78 to 0 deg C, 15 min. E/Z ratio: 68/32;
参考文献
Tetrahedron Letters, , vol. 24, # 24 p. 2481 - 2484
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 30, p. 868 - 875,883 - 889
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 226, p. 1095
反应条件
potassium hydroxide in methanol
参考文献
Otto; Ebner
Archiv der Pharmazie, 1976 , vol. 309, # 12 p. 969 - 978