N-(1-金刚烷基)苯甲酰胺合成路线 （共 22 条）
反应条件
zinc(II) chloride in dichloromethane
96 h; Ambient temperature;
参考文献
Sasaki, Tadashi; Usuki, Arimitsu; Ohno, Masatomi
Journal of Organic Chemistry, 1980 , vol. 45, # 18 p. 3559 - 3564
反应条件
copper(l) iodide; di-tert-butyl peroxide; 4,7-Dimethoxy-1,10-phenanthroline in 1,2-dichloro-benzene
T=100°C; 36 h; Inert atmosphere;
参考文献
Tran, Ba L.; Li, Bijie; Driess, Matthias; Hartwig, John F.
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2555 - 2563
反应条件
2-hydroxy-1,3-isoindolinedione; nitrogen(II) oxide in acetic acid
T=100°C; 20 h; Yield given. Yields of byproduct given;
参考文献
Sakaguchi, Satoshi; Eikawa, Masahiro; Ishii, Yasutaka
Tetrahedron Letters, 1997 , vol. 38, # 40 p. 7075 - 7078
反应条件
1: trichloroacetonitrile; triphenylphosphine / acetonitrile / 0.67 h / 20 °C
2: triethylamine / CH2Cl2 / 20 °C
View Scheme
参考文献
Jang, Doo Ok; Park, Doo Jin; Joonggon, Kim
Tetrahedron Letters, 1999 , vol. 40, # 29 p. 5323 - 5326
反应条件
1: 63 percent / toluene / Heating; azeotropic removal of water
2: 56.2 percent / peroxyacetic acid / CH2Cl2 / 2 h / 0 - 5 °C
3: 91.7 percent / FeSO4*7H2O / methanol / 2 h / Ambient temperature
View Scheme
参考文献
Isaev, S. D.; Novoselov, E. F.; Yurchenko, A. G.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 1 p. 103 - 108
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 1 p. 114 - 119
反应条件
1: 56.2 percent / peroxyacetic acid / CH2Cl2 / 2 h / 0 - 5 °C
2: 91.7 percent / FeSO4*7H2O / methanol / 2 h / Ambient temperature
View Scheme
参考文献
Isaev, S. D.; Novoselov, E. F.; Yurchenko, A. G.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 1 p. 103 - 108
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 1 p. 114 - 119
反应条件
1: 63 percent / toluene / Heating; azeotropic removal of water
2: 56.2 percent / peroxyacetic acid / CH2Cl2 / 2 h / 0 - 5 °C
3: 91.7 percent / FeSO4*7H2O / methanol / 2 h / Ambient temperature
View Scheme
参考文献
Isaev, S. D.; Novoselov, E. F.; Yurchenko, A. G.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 1 p. 103 - 108
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 1 p. 114 - 119
反应条件
1: Mn(III) acetylacetonate / water / 3 h / 70 °C / Inert atmosphere
2: decacarbonyldimanganese (2); hydrogen bromide / water / 5 h / 100 °C / Inert atmosphere
View Scheme
参考文献
Khusnutdinov; Shchadneva; Mayakova, Yu. Yu.; Khisamova; Dzhemilev
Russian Journal of Organic Chemistry, 2011 , vol. 47, # 11 p. 1682 - 1685
反应条件
1: 10 h / Heating
2: aq.potassium carbonate
View Scheme
参考文献
Plakhotnik, V.M.; Kovtun, V.Yu.; Yashunskii, V.G.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 867 - 871
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 1001 - 1005
反应条件
1: 10 h / Heating
2: aq.potassium carbonate
View Scheme
参考文献
Plakhotnik, V.M.; Kovtun, V.Yu.; Yashunskii, V.G.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 867 - 871
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 1001 - 1005
