(2S,3S)-(+)-2,3-丁二醇合成路线 (共 30 条)
反应条件
sodium perchlorate; hydrogen; [(η6-p-cymene)((1S,2S)-N-p-toluenesulfonyl-1,2-diphenylethylenediamine)RuCl] in methanol T=30°C; P=38002.6 Torr; 18 h; Product distribution / selectivity;
参考文献
Nagoya Industrial Science Research Institute
Patent: EP1741693 A1, 2007 ;
Location in patent: Page/Page column 13 ;
反应条件
hydrogen; Pt/Al2O3; cinchonine in toluene P=80256.4 Torr; 1.91667 h; Further byproducts given. Yields of byproduct given;
参考文献
Studer, Martin; Okafor, Victor; Blaser, Hans-Ulrich
Chemical Communications, 1998 , # 9 p. 1053 - 1054
反应条件
recombinant aldo-keto reductase AKR3C1 (Ara1p) from Saccharomyces cerevisiae; NADPH in aq. phosphate buffer T=25°C; pH=7; Enzymatic reaction; Reagent/catalyst; stereospecific reaction;
参考文献
Chemico-Biological Interactions, , vol. 202, # 1-3 p. 195 - 203
反应条件
recombinant human aldo-keto reductase AKR1B10; NADPH in aq. phosphate buffer T=25°C; pH=7; Enzymatic reaction; Reagent/catalyst; stereospecific reaction;
参考文献
Chemico-Biological Interactions, , vol. 202, # 1-3 p. 195 - 203
反应条件
lithium aluminium tetrahydride in diethyl ether 4 h; Heating;
参考文献
Matsumiya, Shigeki; Izuoka, Akira; Sugawara, Tadashi; Taruishi, Tomohiro; Kawada, Yuzo
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 2 p. 513 - 522
反应条件
lithium aluminium tetrahydride
参考文献
Bystroem, Styrbjoern; Hoegberg, Hans-Erik; Norin, Torbjoern
Tetrahedron, 1981 , vol. 37, p. 2249 - 2254
反应条件
potassium carbonate in methanol 1 h; Heating;
参考文献
Liu, Rong; Hoegberg, Hans-Erik
Tetrahedron Asymmetry, 2001 , vol. 12, # 5 p. 771 - 778
反应条件
hydrogen; Pt/Al2O3; cinchonine in toluene P=80256.4 Torr; 1.91667 h; different reaction times; Rate constantProduct distribution;
参考文献
Studer, Martin; Okafor, Victor; Blaser, Hans-Ulrich
Chemical Communications, 1998 , # 9 p. 1053 - 1054
反应条件
(+)-10-camphorsulfonic acid beim Hydratisieren;
参考文献
Journal of the American Chemical Society, , vol. 58, p. 2399
反应条件
D-glucose in water T=33°C; 2 h; Microbiological reaction; optical yield given as percent eestereoselective reaction;
参考文献
Monsalve, Leandro N.; Cerrutti, Patricia; Galvagno, Miguel A.; Baldessari, Alicia
Biocatalysis and Biotransformation, 2010 , vol. 28, # 2 p. 137 - 143