2-羟基-9H-9-氧杂蒽酮合成路线 （共 33 条）
反应条件
1: 85 percent / AlCl3 / CS2 / 4 h / 25 °C
2: 82 percent / Py*HCl / 10 h / 210 °C
View Scheme
参考文献
Han; Bontems; Hegyes; Munson; Minor; Kates; Albericio; Barany
Journal of Organic Chemistry, 1996 , vol. 61, # 18 p. 6326 - 6339
反应条件
1: 85 percent / AlCl3 / CS2 / 4 h / 25 °C
2: 82 percent / Py*HCl / 10 h / 210 °C
View Scheme
参考文献
Han; Bontems; Hegyes; Munson; Minor; Kates; Albericio; Barany
Journal of Organic Chemistry, 1996 , vol. 61, # 18 p. 6326 - 6339
反应条件
1: 70 percent / K2CO3; Cu; CuI / Clealand's reagent / dimethylformamide / 6 h / Heating
2: 90 percent / Ac2O; H2SO4 / 1 h / 80 °C
3: 97 percent / 2,6-lutidine; LiI / 48 h / Heating
View Scheme
参考文献
Somlai, Csaba; Hegyes, Peter; Fenyoe, Robert; Toth, Gabor K.; Penke, Botond; Voelter, Wolfgang
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2001 , vol. 56, # 6 p. 526 - 532
反应条件
1: 70 percent / K2CO3; Cu; CuI / Clealand's reagent / dimethylformamide / 6 h / Heating
2: 90 percent / Ac2O; H2SO4 / 1 h / 80 °C
3: 97 percent / 2,6-lutidine; LiI / 48 h / Heating
View Scheme
参考文献
Somlai, Csaba; Hegyes, Peter; Fenyoe, Robert; Toth, Gabor K.; Penke, Botond; Voelter, Wolfgang
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2001 , vol. 56, # 6 p. 526 - 532
参考文献
Oleinik, A. F.; Adamskaya, E. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 11 p. 1221 - 1224
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 11 p. 1537 - 1539
参考文献
Lamb; Suschitzky
Tetrahedron, 1959 , vol. 5, p. 1,7
参考文献
Lamb; Suschitzky
Tetrahedron, 1959 , vol. 5, p. 1,7
反应条件
1: 71 percent
2: 80 percent / AlCl3 / benzene / Heating
3: 73 percent / Cu
View Scheme
参考文献
Oleinik, A. F.; Adamskaya, E. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 11 p. 1221 - 1224
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 11 p. 1537 - 1539
反应条件
1: 80 percent / AlCl3 / benzene / Heating
2: 73 percent / Cu
View Scheme
参考文献
Oleinik, A. F.; Adamskaya, E. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 11 p. 1221 - 1224
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 11 p. 1537 - 1539
反应条件
1: potassium hydroxide / ethanol / 72 h / Reflux
2: hydrogen bromide / Inert atmosphere; Reflux
View Scheme
参考文献
Qu, Ruijuan; Zhang, Qi; Zhang, Xuesheng; Wang, Zunyao
Spectroscopy Letters, 2012 , vol. 45, # 4 p. 240 - 245
