3,4,5-三甲氧基苯甲酸甲酯合成路线 （共 184 条）
反应条件
1: lithium aluminium hydride / diethyl ether / 3 h / Heating
2: pyridinium chlorochromate / CH2Cl2 / 3 h
3: sodium acetate / acetic anhydride / Heating
4: NaOH / H2O / Heating
View Scheme
参考文献
Shaw; Srivastava; Jha
Journal of the Indian Chemical Society, 1990 , vol. 67, # 2 p. 144 - 147
反应条件
1: Cu(NO3)2, Ac2O
2: (alkaline hydrolysis)
3: NaBH4, BF3-Et2O
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参考文献
Williams,K.I.H. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 3982 - 3988
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran
2: thionyl chloride / dichloromethane
3: potassium carbonate / dimethyl sulfoxide / 6 h / 50 °C
4: sodium chloride / dimethyl sulfoxide / 5 h / |Reflux
5: lithium aluminium tetrahydride / tetrahydrofuran / 2.5 h / 20 °C / |Reflux
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参考文献
Zheng, Cheng; Guo, Yibing; Meng, Ying; Dou, Sufeng; Shao, Jian; Yang, Yumin
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 5 p. 654 - 664
反应条件
1: sodium / 140 °C
2: hydriodic acid
View Scheme
参考文献
Bargellini; Monti
Gazzetta Chimica Italiana, 1915 , vol. 45 I, p. 68
