3,4,5-三甲氧基苯甲酸甲酯合成路线 (共 184 条)
反应条件
sodium methylate in methanol T=20°C; Hydrolysis; 1 h;
参考文献
Phytochemistry, , vol. 52, # 3 p. 445 - 452
反应条件
toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid in acetonitrile T=80°C; Baeyer-Villiger oxidation; 2 h; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 70, # 18 p. 7290 - 7296
反应条件
in ethanol; dichloromethane T=0°C;
参考文献
Liebigs Annalen der Chemie, , p. 401 - 404
反应条件
1: C55H58O28 With sodium hydroxide in methanol T=70°C; 0.5 h; 2: diazomethane in diethyl ether Further stages.;
参考文献
Journal of Natural Products, , vol. 64, # 12 p. 1527 - 1532
反应条件
1: C65H68O33 With sodium hydroxide in methanol T=70°C; 1 h; 2: diazomethane in methanol T=0°C; 2 h;
参考文献
Journal of Natural Products, , vol. 67, # 6 p. 1018 - 1022
反应条件
1: in diethyl ether; ethanol T=20°C; 8 h; 2: With sodium methylate in methanol T=20°C; 4 h;
参考文献
Phytochemistry, , vol. 69, # 18 p. 3080 - 3086
反应条件
tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate in toluene 6 h; Heating;
参考文献
Journal of Medicinal Chemistry, , vol. 38, # 12 p. 2130 - 2137
反应条件
1: nobotanin O; dimethyl sulfate With potassium carbonate in acetone Methylation; rt, overnight; reflux, 3 h; 2: methanol With sodium hydroxide T=20°C; methanolysis; 6 h;
参考文献
Phytochemistry, , vol. 52, # 8 p. 1661 - 1666
反应条件
1: in diethyl ether; ethanol T=20°C; 2: With methanol; sodium methylate T=20°C;
参考文献
Journal of Agricultural and Food Chemistry, , vol. 55, # 3 p. 672 - 679
反应条件
1: bergecin A With trifluoroacetic acid in water 40 h; Reflux; 2: diazomethane in diethyl ether T=4°C; 3 h;
参考文献
Chemistry and Biodiversity, , vol. 9, # 1 p. 91 - 98