3,4,5-三甲氧基苯甲酸甲酯合成路线 （共 184 条）
反应条件
1.1: 98 percent / NaCN; MnO2 / propan-2-ol; CHCl3 / 2 h / 20 °C 2.1: Na2HPO4 / acetonitrile / 20 °C 2.2: 87 percent / aq. NaHCO3 / 18 h View Scheme
参考文献
Tetrahedron, , vol. 56, # 51 p. 9875 - 9883
反应条件
1.1: pyridine / CH2Cl2 / 20 h 2.1: Na2HPO4 / acetonitrile / 20 °C 2.2: 95 percent / aq. NaHCO3 / 18 h View Scheme
参考文献
Tetrahedron, , vol. 56, # 51 p. 9875 - 9883
反应条件
hydrogenchloride; n-butyllithium; CuI*[P(OEt3)] Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 102, # 2 p. 790 - 798
反应条件
sodium methylate in methanol 20 h; Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 38, # 6 p. 1518 - 1523
反应条件
sodium methylate in methanol 0.5 h; Ambient temperature;
参考文献
Chemical and pharmaceutical bulletin, , vol. 37, # 8 p. 2063 - 2070
反应条件
1: 13.6 percent / 7percent NaOH aq. / aq. ethanol / 10 h / Heating; var. condition 2: 0.21 g / K2CO3 / acetone / 4 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 9 p. 3039 - 3055
反应条件
sodium hydroxide in methanol 1 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 38, # 5 p. 1218 - 1223
反应条件
sodium methylate in methanol Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 37, # 10 p. 2655 - 2660
反应条件
potassium carbonate in N,N-dimethyl-formamide 7 h; Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 9 p. 3024 - 3038
反应条件
potassium carbonate in acetone 4 h; Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 9 p. 3039 - 3055
