3,4,5-三甲氧基苯甲酸甲酯合成路线 (共 184 条)
反应条件
potassium carbonate in acetone 12 h; Heating; Further byproducts given;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 6 p. 351 - 353
反应条件
sodium methylate 1.) ethanol, ether, room temperature, overnight, 2.) methanol, room temperature, overnight; Multistep reaction;
参考文献
Phytochemistry, , vol. 50, # 2 p. 307 - 312
参考文献
Monatshefte fuer Chemie, , vol. 33, p. 846,847
反应条件
sodium hydroxide 1.) MeOH, reflux, 1 h; 2.) ether, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 37, # 1 p. 129 - 134
反应条件
copper bronze 1.) from 240 deg C to 280 deg C, 2.) 280 deg C, 20 min;
参考文献
Australian Journal of Chemistry, , vol. 34, # 4 p. 799 - 817
反应条件
in methanol 20 h; Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 34, # 3 p. 1039 - 1049
反应条件
sodium hydroxide; potassium carbonate 1) Me2CO, reflux, 2 h; 2) MeOH, 90 deg C, 1 h; 3) Et2O; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Phytochemistry, , vol. 38, # 2 p. 509 - 513
反应条件
sodium methylate Multistep reaction;
参考文献
Phytochemistry, , vol. 40, # 2 p. 555 - 561
反应条件
sodium hydroxide 1.) methanol, reflux, 1 h, 2.) ether, room temperature; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 38, # 7 p. 1844 - 1851
反应条件
1: HCl, H2O / 1.) 100 deg C, 14 h, 2.) r.t., 8 h 2: BF3 / 3 h / Heating View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 18 p. 2979 - 2987