1-甲基-4,5-二硝基-咪唑合成路线 （共 9 条）
反应条件
NO2OTf in nitromethane T=95°C; 2.5 h;
参考文献
Duddu, Raja; Zhang, Mao-Xi; Damavarapu, Reddy; Gelber, Nathaniel
Synthesis, 2011 , # 17 art. no. M43211SS, p. 2859 - 2864
反应条件
sodium hydrogencarbonate 2 h; Ambient temperature;
参考文献
Suwinski, Jerzy; Salwinska, Ewa; Watras, Jan; Widel, Maria
Polish Journal of Chemistry, 1982 , vol. 56, # 10-12 p. 1261 - 1272
反应条件
in diethyl ether Ambient temperature;
参考文献
Suwinski, Jerzy; Salwinska, Ewa; Watras, Jan; Widel, Maria
Polish Journal of Chemistry, 1982 , vol. 56, # 10-12 p. 1261 - 1272
反应条件
nitronium tetrafluoroborate in nitromethane T=-20 - 125°C;
参考文献
Duddu, Raja; Zhang, Mao-Xi; Damavarapu, Reddy; Gelber, Nathaniel
Synthesis, 2011 , # 17 art. no. M43211SS, p. 2859 - 2864
反应条件
sulfuric acid; anhydrous lithium nitrate; nitric acid T=20 - 120°C;
参考文献
Duddu, Raja; Zhang, Mao-Xi; Damavarapu, Reddy; Gelber, Nathaniel
Synthesis, 2011 , # 17 art. no. M43211SS, p. 2859 - 2864
反应条件
sulfuric acid; anhydrous lithium nitrate; nitric acid T=20 - 120°C;
参考文献
Duddu, Raja; Zhang, Mao-Xi; Damavarapu, Reddy; Gelber, Nathaniel
Synthesis, 2011 , # 17 art. no. M43211SS, p. 2859 - 2864
反应条件
hydrogenchloride 3 h; Heating;
参考文献
Suwinski, Jerzy; Salwinska, Ewa; Watras, Jan; Widel, Maria
Polish Journal of Chemistry, 1982 , vol. 56, # 10-12 p. 1261 - 1272
反应条件
in ethanol T=20°C; 2 h; regioselective reaction;
参考文献
Zaprutko, Lucjusz; Zwawiak, Justyna; Olender, Dorota; Gzella, Andrzej
Heterocycles, 2012 , vol. 85, # 9 p. 2197 - 2211
反应条件
in tetrahydrofuran
T=20°C; 24 h; regioselective reaction;
参考文献
Zaprutko, Lucjusz; Zwawiak, Justyna; Olender, Dorota; Gzella, Andrzej
Heterocycles, 2012 , vol. 85, # 9 p. 2197 - 2211
