三乙二醇二(对甲苯磺酸酯)合成路线 （共 90 条）
反应条件
potassium iodide in acetone T=40°C;
参考文献
Aoki, Yuko; Umezawa, Naoki; Asano, Yuko; Hatano, Keiichiro; Yano, Yuki; Kato, Nobuki; Higuchi, Tsunehiko
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 22 p. 7108 - 7115
反应条件
sodium hydride in tetrahydrofuran T=25°C;
参考文献
Journal of Organic Chemistry, , vol. 59, # 8 p. 2186 - 2196
反应条件
aluminum oxide; potassium fluoride in acetonitrile 72 h; Ambient temperature;
参考文献
Yamawaki, Junko; Ando, Takashi
Chemistry Letters, 1980 , p. 533 - 536
反应条件
potassium hydroxide; ammonium hydroxide in 1,4-dioxane 1) 5 days 2) overnight;
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, p. 1077 - 1083
反应条件
aluminum oxide; potassium fluoride in acetonitrile 24 h; Ambient temperature;
参考文献
Yamawaki, Junko; Ando, Takashi
Chemistry Letters, 1980 , p. 533 - 536
反应条件
sodium t-butanolate in 1,4-dioxane; tert-butyl alcohol T=40°C; 2.5 h;
参考文献
Maeda, Hirokazu; Kikui, Takashi; Nakatsuji, Yohji; Okahara, Mitsuo
Journal of Organic Chemistry, 1982 , vol. 47, # 26 p. 5167 - 5171
反应条件
1: 98 percent / NaH / tetrahydrofuran / 24 h 2: 92 percent / H2 / Pd/C / CH2Cl2 / 48 h / 20 °C / 38000 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 64, # 18 p. 6870 - 6873
反应条件
potassium hydroxide 1.) 50 deg C, 0.1 mm Hg, 5 h, 2.) THF, room temperature, 10 d; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society - Faraday Transactions, , vol. 92, # 17 p. 3173 - 3182
反应条件
sodium hydride in tetrahydrofuran 24 h; Heating;
参考文献
Tetrahedron Letters, , vol. 48, # 38 p. 6633 - 6636
反应条件
sodium carbonate in acetonitrile Heating;
参考文献
Sakamoto, Hidefumi; Kimura, Keiichi; Koseki, Yasuaki; Matsuo, Mitsunori; Shono, Toshiyuki
Journal of Organic Chemistry, 1986 , vol. 51, # 25 p. 4974 - 4979
