in neat (no solvent) (N2); mixing of NaN(CN)2 and CBr4 in agate mortar in 1:4 ratio; grindingfor 5 min; placing in Cu container; pressing at 300 kg/cm**2 for 5 min; shock treatment (14 GPa); washing with water; monitoring by XRD;
参考文献
Shibata, Kazusato; Sekine, Toshimori
Solid State Communications, 2006 , vol. 139, # 10 p. 501 - 505
in neat (no solvent) (N2); mixing of NaN(CN)2 and CI4 in agate mortar in 1:4 ratio; grinding for 5 min; placing in Cu container; pressing at 300 kg/cm**2 for 5 min; shock treatment (21 GPa); monitoring by XRD;
参考文献
Shibata, Kazusato; Sekine, Toshimori
Solid State Communications, 2006 , vol. 139, # 10 p. 501 - 505
1: piperidine With hydrogenchloride in water; butan-1-ol T=0°C; 0.5 h; 2: sodium dicyanoamide in water; butan-1-ol 24 h; Reflux;
参考文献
HANALL BIOPHARMA CO., LTD.; KIM, Sung Wuk; MIN, Chang Hee; PARK, Se Hwan; KIM, Duck; LEE, Ji Sun; KIM, Yong Eun; OH, Ju Hoon
Patent: WO2013/22278 A2, 2013 ;
Location in patent: Paragraph 101-103 ;
WO 2013/022278 A2
