4,5,6,7-四氢-5-甲基-1,3-异苯并呋喃二酮合成路线 （共 7 条）
反应条件
Erhitzen des Reaktionsprodukts auf 210grad;
参考文献
Craig
Journal of the American Chemical Society, 1950 , vol. 72, p. 3732
反应条件
1,3-bis-(diphenylphosphino)propane; acetic acid; triethylamine; palladium dichloride
T=120°C; P=7600.51 Torr; 3 h; Autoclave;
参考文献
Bae, Yeon Kyu; Cho, Chan Sik
Synlett, 2013 , vol. 24, # 14 art. no. ST-2013-U0446-L, p. 1848 - 1850
反应条件
in acetic anhydride; toluene
参考文献
Merck Sharp and Dohme Limited
Patent: US6255305 B1, 2001 ;
US 6255305 B1
反应条件
hydrogen; aluminium containing platinum black
T=150°C; 2.5 h; effect of further catalysts and various catalyst concentration, effect of operation time and temperature; Product distribution;
参考文献
Sibarov, D. A.; Dokuchaeva, T. G.; Lezdin, S. Yu.; Silin, A. A.
J. Appl. Chem. USSR (Engl. Transl.), 1988 , vol. 61, # 9 p. 2060 - 2063,1863 - 1866
参考文献
Craig
Journal of the American Chemical Society, 1950 , vol. 72, p. 3732
Full Text View citing articles Show Details
Wicks et al.
Journal of Organic Chemistry, 1947 , vol. 12, p. 713,716
反应条件
1: phosphorus tribromide
2: sodium chlorite; dihydrogen peroxide
3: palladium dichloride; 1,3-bis-(diphenylphosphino)propane; triethylamine; acetic acid / 3 h / 120 °C / 7600.51 Torr / |Autoclave
View Scheme
参考文献
Bae, Yeon Kyu; Cho, Chan Sik
Synlett, 2013 , vol. 24, # 14 art. no. ST-2013-U0446-L, p. 1848 - 1850
反应条件
hydrogen; 5 Ni/Al2O3
T=450°C; further catalysts, further temperature; Product distribution;
参考文献
Dokuchaeva; Lezdin; Libarov; Paduto
Journal of applied chemistry of the USSR, 1985 , vol. 58, # 9 pt 2 p. 1894 - 1900
