3-氨基-2-苯基二氢茚酮合成路线 （共 10 条）
反应条件
lithium diisopropyl amide in tetrahydrofuran T=-10 - 20°C; Cyclization;
参考文献
Journal of Organic Chemistry, , vol. 65, # 15 p. 4515 - 4522
反应条件
ammonium hydroxide in ethanol
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 2453 - 2460
反应条件
lithium diisopropyl amide in tetrahydrofuran T=-10 - 20°C;
参考文献
Tetrahedron Letters, , vol. 38, # 47 p. 8121 - 8124
反应条件
hydrogenchloride in methanol 1 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 39, # 1 p. 131 - 135
反应条件
1: 75 percent / NaH / tetrahydrofuran / Heating 2: 64 percent / LDA / tetrahydrofuran / -10 - 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 15 p. 4515 - 4522
反应条件
1: 75 percent / NaH / tetrahydrofuran / Heating 2: 64 percent / LDA / tetrahydrofuran / -10 - 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 15 p. 4515 - 4522
反应条件
1: 31 percent / triethylamine / acetic anhydride / 0.5 h / Heating 2: 88 percent / phosphoroxychloride / 4 h / Heating 3: 97 percent / sodium azide / acetonitrile / 0.5 h / 0 °C 4: 90 percent / toluene / 30 h / 20 °C 5: 48 percent / aq. hydrochloric acid / methanol / 1 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 39, # 1 p. 131 - 135
反应条件
1: 97 percent / sodium azide / acetonitrile / 0.5 h / 0 °C 2: 90 percent / toluene / 30 h / 20 °C 3: 48 percent / aq. hydrochloric acid / methanol / 1 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 39, # 1 p. 131 - 135
反应条件
1: 90 percent / toluene / 30 h / 20 °C 2: 48 percent / aq. hydrochloric acid / methanol / 1 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 39, # 1 p. 131 - 135
参考文献
Zhurnal Obshchei Khimii, , vol. 27, p. 2509,2512
J. Gen. Chem. USSR (Engl. Transl.), , vol. 27, p. 2567,2570
