1-甲基-1H-咪唑-4,5-二羧酸合成路线 (共 17 条)
反应条件
potassium hydroxide 9 h; Heating;
参考文献
Bierer, Donald E.; O'Connell, John F.; Parquette, Jon R.; Thompson, Charles M.; Rapoport, Henry
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1390 - 1405
反应条件
1: 90 percent / sodium hydrogen carbonate / H2O 2: 75 percent / sodium hydroxide / Heating View Scheme
参考文献
Organic Letters, , vol. 8, # 5 p. 923 - 926
反应条件
1: aqueous HNO3 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 74, p. 1084
参考文献
Journal of the American Chemical Society, , vol. 74, p. 1084
反应条件
1: NaOMe / methanol 2: aq. KOH / ethanol / 2 h View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , p. 364 - 367
Zhurnal Organicheskoi Khimii, , vol. 19, # 2 p. 416 - 420
参考文献
Zhurnal Obshchei Khimii, , vol. 26, p. 455,456; engl. Ausg. S. 479, 480
反应条件
N,N-dimethyl acetamide T=180°C; 3 h;
参考文献
O'Connell, John F.; Parquette, Jonathan; Yelle, William E.; Wang, Wilhelm; Rapoport, Henry
Synthesis, 1988 , # 10 p. 767 - 771
反应条件
acetic anhydride T=95 - 100°C; Title compound not separated from byproducts;
参考文献
Collman, James P.; Yan, Yi-Long; Lei, Jianping; Dinolfo, Peter H.
Organic Letters, 2006 , vol. 8, # 5 p. 923 - 926
反应条件
acetic anhydride T=100°C; 4 h;
参考文献
Takahashi, Kazuyuki; Mitsuhashi, Keiryo
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 2 p. 557 - 558
反应条件
acetic anhydride T=95 - 100°C; Title compound not separated from byproducts;
参考文献
Collman, James P.; Yan, Yi-Long; Lei, Jianping; Dinolfo, Peter H.
Organic Letters, 2006 , vol. 8, # 5 p. 923 - 926