N-叔丁基=4-甲氧基苯甲酰胺合成路线 (共 29 条)
反应条件
1: sodium nitrite / acetic anhydride; acetic acid / 3 h / 0 °C 2: acetic anhydride; acetic acid / 16 h / 20 °C View Scheme
参考文献
Le, Hoang V.; Fan, Lijun; Ganem, Bruce
Tetrahedron Letters, 2011 , vol. 52, # 17 p. 2209 - 2211
反应条件
scandium tris(trifluoromethanesulfonate) in nitromethane T=170°C; 1 h; Irradiation;
参考文献
Mahalingam; Wu, Xiongyu; Alterman, Mathias
Tetrahedron Letters, 2006 , vol. 47, # 18 p. 3051 - 3053
反应条件
[BMIM(SO3H)][OTf]
T=50°C; Ritter reaction; 3 h; Inert atmosphereIonic liquid;
参考文献
Kalkhambkar, Rajesh G.; Waters, Sarah N.; Laali, Kenneth K.
Tetrahedron Letters, 2011 , vol. 52, # 8 p. 867 - 871
反应条件
sulfuric acid
T=42°C; 2 h;
参考文献
Reddy, K. Laxma
Tetrahedron Letters, 2003 , vol. 44, # 7 p. 1453 - 1455
反应条件
sodium hydroxide in dichloromethane
参考文献
Clayden, Jonathan; Hebditch, Katherine R.; Read, Benjamin; Helliwell, Madeleine
Tetrahedron Letters, 2007 , vol. 48, # 48 p. 8550 - 8553
反应条件
triethylamine; palladium diacetate; triphenylphosphine in toluene
T=60°C; P=750.06 Torr; 8 h;
参考文献
Takacs, Eszter; Varga, Csilla; Skoda-Foeldes, Rita; Kollar, Laszlo
Tetrahedron Letters, 2007 , vol. 48, # 14 p. 2453 - 2456
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide
T=90°C;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide
T=90°C;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031
反应条件
air; 1,8-diazabicyclo[5.4.0]undec-7-ene; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II) in tetrahydrofuran
T=150°C; 0.25 h;
参考文献
Wannberg, Johan; Larhed, Mats
Journal of Organic Chemistry, 2003 , vol. 68, # 14 p. 5750 - 5753
反应条件
N,N,N',N,-tetramethylethylenediamine; di-(1-adamantyl)-n-butylphosphine; palladium diacetate in toluene
T=115°C; P=26252.1 Torr; 16 h;
参考文献
Neumann, Helfried; Brennfuehrer, Anne; Gross, Peter; Riermeier, Thomas; Almena, Juan; Beller, Matthias
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 10-11 p. 1255 - 1261