N-叔丁基=4-甲氧基苯甲酰胺合成路线 （共 29 条）
反应条件
triethylamine in dichloromethane
T=20°C; 1 h;
参考文献
Kang, Dong Ho; Joo, Tae Young; Lee, Eun Hwa; Chaysripongkul, Skaydaw; Chavasiri, Warinthorn; Jang, Doo Ok
Tetrahedron Letters, 2006 , vol. 47, # 32 p. 5693 - 5696
反应条件
1: palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; sodium acetate; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4; N,N-dicyclohexylmethylamine / ethylene glycol dimethyl ether / 18 h / 85 °C
2: pyridine; triethylamine / 26 h / 70 °C
View Scheme
参考文献
Burhardt, Mia N.; Taaning, Rolf H.; Skrydstrup, Troels
Organic Letters, 2013 , vol. 15, # 4 p. 948 - 951
反应条件
1: hydrofluoroboric acid; sodium nitrite / water / 0.58 h / 0 °C
2: caesium carbonate; water / acetone / 0.33 h / 0 °C / |Schlenk technique; |Inert atmosphere
View Scheme
参考文献
Xia, Zhonghua; Zhu, Qiang
Organic Letters, 2013 , vol. 15, # 16 p. 4110 - 4113
反应条件
AcOH-d4; sulfuric acid
T=20°C; Inert atmosphereEnzymatic reaction;
参考文献
Baum, Jean C.; Milne, Jacqueline E.; Murry, Jerry A.; Thiel, Oliver R.
Journal of Organic Chemistry, 2009 , vol. 74, # 5 p. 2207 - 2209
反应条件
1: triethylamine / dichloromethane / 20 °C / |Inert atmosphere
2: lithium aluminium tetrahydride
View Scheme
参考文献
Kim, Jiyu; Kim, Jinwoo; Chang, Sukbok
Chemistry - A European Journal, 2013 , vol. 19, # 23 p. 7328 - 7333
反应条件
potassium tert-butylate; ammonium chloride
1.) THF, reflux, 2 h; Yield given. Multistep reaction;
参考文献
Aitken, R. Alan; Raut, Swati V.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 7 p. 747 - 751
反应条件
lithium aluminium tetrahydride
参考文献
Kim, Jiyu; Kim, Jinwoo; Chang, Sukbok
Chemistry - A European Journal, 2013 , vol. 19, # 23 p. 7328 - 7333
反应条件
Ambient temperatureseveral months;
参考文献
Paredes, Rodrigo; Bastos, Holger; Montoya, Raul; Chavez, Alba Lucia; Dolbier, William R.; Burkholder, Conrad R.
Tetrahedron, 1988 , vol. 44, # 22 p. 6821 - 6830
反应条件
in ethanol
1.5 h; Irradiation; Quantum yield;
参考文献
Ogata, Yoshiro; Tagaki, Katsuhiko; Mizuno, Kiyohiko
Journal of Organic Chemistry, 1982 , vol. 47, p. 3684 - 3687
