3,5-二(4-氨基苯氧基)苯甲酸合成路线 (共 5 条)
反应条件
hydrogen; palladium on activated charcoal in ethanol; acetone P=3102.89 - 3361.46 Torr; 24 h;
参考文献
Baek, Jong-Beom; Ferguson, John B.; Tan, Loon-Seng
Macromolecules, 2003 , vol. 36, # 12 p. 4385 - 4396
反应条件
1: 91 percent / potassium carbonate / 1-methyl-pyrrolidin-2-one / 8 h / 120 - 140 °C 2: 83.7 percent / H2 / Pd/C / ethanol; acetone / 24 h / 3102.89 - 3361.46 Torr View Scheme
参考文献
Macromolecules, , vol. 36, # 12 p. 4385 - 4396
反应条件
1: 91 percent / potassium carbonate / 1-methyl-pyrrolidin-2-one / 8 h / 120 - 140 °C 2: 83.7 percent / H2 / Pd/C / ethanol; acetone / 24 h / 3102.89 - 3361.46 Torr View Scheme
参考文献
Macromolecules, , vol. 36, # 12 p. 4385 - 4396
反应条件
1: acetic acid With DBOP; triethylamine in 1-methyl-pyrrolidin-2-one
T=20°C; 1 h;
2: 3,5-bis(4-aminophenyloxy)benzoic acid in 1-methyl-pyrrolidin-2-one
1 h;
参考文献
Okazaki, Masaki; Washio, Isao; Shibasaki, Yuji; Ueda, Mitsuru
Journal of the American Chemical Society, 2003 , vol. 125, # 27 p. 8120 - 8121
反应条件
in 1-methyl-pyrrolidin-2-one
T=0°C; 3 h;
参考文献
Washio, Isao; Shibasaki, Yuji; Ueda, Mitsuru
Organic Letters, 2003 , vol. 5, # 22 p. 4159 - 4161
Title/Abstract Full Text View citing articles Show Details
Washio, Isao; Shibasaki, Yuji; Ueda, Mitsuru
Macromolecules, 2005 , vol. 38, # 6 p. 2237 - 2246