1-(4-氯苯基)-乙酮肟合成路线 （共 37 条）
反应条件
sodium hydrogen sulphate monohydrate; [MoCl5]; sodium cyanoborohydride in ethanol 1 h; Reflux;
参考文献
Kouhkan, Mehri; Zeynizadeh, Behzad
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 9 p. 3323 - 3326
参考文献
Lyle; Troscianiec
Journal of Organic Chemistry, 1955 , vol. 20, p. 1757,1758,1759
反应条件
1: 69 percent / imidazole / dimethylformamide / 80 - 120 °C 2: 1.) BH3*THF, 2.) aq. HCl / 1.) reflux, 8 h, 2.) 50 deg C, 2 h View Scheme
参考文献
Lyle; Troscianiec
Journal of Organic Chemistry, 1955 , vol. 20, p. 1757,1758,1759
参考文献
Lyle; Troscianiec
Journal of Organic Chemistry, 1955 , vol. 20, p. 1757,1758,1759
反应条件
hydrogen bromide; dihydrogen peroxide in water; acetic acid T=15 - 106°C; 0.333333 h;
参考文献
Terentev, Alexander O.; Krylov, Igor B.; Vil, Vera A.; Pastukhova, Zhanna Yu.; Fastov, Sergey A.; Nikishin, Gennady I.
Central European Journal of Chemistry, 2012 , vol. 10, # 2 p. 360 - 367
反应条件
lithium hydroxide in dimethyl sulfoxide
T=100°C; P=9120 Torr; 3 h;
参考文献
Korostova, S. E.; Sobenina, L. N.; Nesterenko, R. N.; Aliev, I. A.; Mikhaleva, A. I.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1790 - 1793
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 9 p. 1960 - 1964
反应条件
potassium hydroxide; water in dimethyl sulfoxide
T=70 - 80°C; P=8360 Torr; 6 h;
参考文献
Tarasova, O. A.; Korostova, S. E.; Mikhaleva, A. I.; Sobenina, L. N.; Nesterenko, R. N.; et al.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 6.1 p. 863 - 869
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 6 p. 810 - 815
反应条件
potassium hydroxide in dimethyl sulfoxide
T=50°C; P=10640 Torr; 3 h;
参考文献
Korostova, S. E.; Mikhaleva, A. I.; Sobenina, L. N.; Shevchenko, S. G.; Shcherbakov, V. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1985 , vol. 21, # 11 p. 1238 - 1241
Khimiya Geterotsiklicheskikh Soedinenii, 1985 , vol. 21, # 11 p. 1501 - 1505
反应条件
potassium hydroxide in dimethyl sulfoxide
T=120°C; 6 h;
参考文献
Korostova, S. E.; Mikhaleva, A. I.; Sobenina, L. N.; Shevchenko, S. G.; Polovnikova, R. I.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, p. 436 - 438
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 3 p. 492 - 495
反应条件
lithium diisopropyl amide
1) THF, 0 deg C, 45 min.; 2) 60 min.; Yield given. Multistep reaction;
参考文献
Park, Dorothy J.; Fulmer, Tammy D.; Beam, Charles F.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 649 - 652
