1: With sulfuric acid; sodium nitrite in water; dimethyl sulfoxide T=5°C; Sandmeyer Reaction; 2: With sodium iodide in water; dimethyl sulfoxide T=5 - 20°C;

iodine; acetic acid; mercury(II) oxide

iodine; thallous acetate in dichloromethane 48 h; Ambient temperature;

iodine in dichloromethane 24 h; Ambient temperature; Further byproducts given;

iodine in dichloromethane 24 h; Ambient temperature; Further byproducts given;

iodine cloride in water T=25°C; pH=4.8; Kinetics; regiospecific reaction;

暂无反应条件数据

暂无反应条件数据

durch Methylierung;

1: potassium carbonate / acetone / 6 h / 20 °C / |Reflux 2: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / acetonitrile / |Inert atmosphere; |Reflux 3: sodium hydrogencarbonate; magnesium sulfate; sodium periodate; ruthenium trichloride / acetonitrile; tetrachloromethane; water / 2 h / 20 °C 4: 1,8-diazabicyclo[5.4.0]undec-7-ene / dimethyl sulfoxide / 1 h / 100 °C View Scheme