2,4-二甲基-3-戊醇合成路线 （共 16 条）
反应条件
1: phosphorus (III)-bromide 2: diethyl ether / Erwaermen des nach Abdestillieren des Loesungmittels erhaltenen Reaktionsgemisches auf 60-70grad View Scheme
参考文献
Tschel'zowa et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 522,526; engl.Ausg.S. 459, 462
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; tetra-n-butylammonium perchlorate
T=0°C; current density = 25 mA/cm2, 2.0 F/mol of halide;
参考文献
Satoh; Suginome; Tokuda
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 6 p. 1791 - 1794
反应条件
bei der Destillation unter gewoehnlichem Druck;
参考文献
Lemaire
Recueil des Travaux Chimiques des Pays-Bas, 1910 , vol. 29, p. 59
Chem. Zentralbl., 1909 , vol. 80, # I p. 1982
反应条件
potassium cyanide; ethanol
参考文献
Franke
Monatshefte fuer Chemie, 1913 , vol. 34, p. 1904
参考文献
Kieffer,R.
Bulletin de la Societe Chimique de France, 1967 , p. 3026 - 3029
反应条件
(i) nBuLi, KOtBu, hexane, pentane, (ii) /BRN= 635680/, THF; Multistep reaction;
参考文献
Bates,R.B. et al.
Journal of Organic Chemistry, 1979 , vol. 44, p. 3800 - 3803
反应条件
sodium tetrahydroborate; Hg(NO3)2
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bloodworth, A. J.; Khan, Jamil A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2450 - 2457
反应条件
molybdenium(VI) oxotetrachloride
1) THF, -35 deg C, 1 h, 2) THF, -35 -> 20 deg C, 18 h; Yield given. Multistep reaction;
参考文献
Kauffmann, Thomas; Fiegenbaum, Petra; Papenberg, Michael; Wieschollek, Raphael; Wingbermuehle, Dorothea
Chemische Berichte, 1993 , vol. 126, # 1 p. 79 - 88
反应条件
(i) pentane, (ii) H2NCH2CH2OH; Multistep reaction;
参考文献
Kramer,G.W.; Brown,H.C.
Journal of Organic Chemistry, 1977 , vol. 42, p. 2292 - 2299
反应条件
(i), (ii) (HOCH2CH2)3N; Multistep reaction;
参考文献
Mikhailov,B.M. et al.
Journal of Organometallic Chemistry, 1978 , vol. 154, p. 131 - 145
