2,3,5,6-四氟苯甲醛合成路线 (共 14 条)
反应条件
formic acid; nickel monoaluminide in methanol; water
参考文献
Showa Denko K.K.
Patent: US6020517 A1, 2000 ;
反应条件
acetic acid; nickel monoaluminide in 1,4-dioxane; water
参考文献
Showa Denko K.K.
Patent: US6020517 A1, 2000 ;
反应条件
acetic acid; nickel monoaluminide in methanol; water
参考文献
Showa Denko K.K.
Patent: US6020517 A1, 2000 ;
反应条件
hydrogen; sulfuric acid; nickel; copper(II) sulfate in water T=20 - 60°C; 0.5 h;
参考文献
Showa Denko K K
Patent: EP1182184 A1, 2002 ;
Location in patent: Page 13 ;
反应条件
4-(N,N-dimethlyamino)pyridine; C21H27AuN2 in dichloromethane T=40°C; 12 h; Inert atmosphere;
参考文献
Lv, Hongbin; Zhan, Jin-Hui; Cai, Yuan-Bo; Yu, Yi; Wang, Bingwu; Zhang, Jun-Long
Journal of the American Chemical Society, 2012 , vol. 134, # 39 p. 16216 - 16227,12
反应条件
water; sulfuric acid in water T=25°C; 1 h;
参考文献
Showa Denko K K
Patent: EP1182184 A1, 2002 ;
Location in patent: Page 10 ;
反应条件
sulfuric acid in dichloromethane; water
反应条件
1: 1,2,4,5-tetrafluorobenzene With n-butyllithium in tetrahydrofuran T=-50°C; 1 h; 2: formic acid ethyl ester in tetrahydrofuran T=-50 - 20°C;
参考文献
Journal of Fluorine Chemistry, , vol. 120, # 1 p. 77 - 84
反应条件
acetic acid; nickel monoaluminide in 1,4-dioxane; water
参考文献
Showa Denko K.K.
Patent: US6020517 A1, 2000 ;
参考文献
Showa Denko K.K.
Patent: US6624336 B1, 2003 ;