1,2-o-异亚丙基-3-苄氧基-5,6-二脱氧-呋喃葡萄糖合成路线 （共 19 条）
反应条件
1: pyridine / CH2Cl2 / 1 h / 0 °C
2: 37 percent / tris(dimethylamino)sulfonium difluorotrimethylsilicate (TASF) / CH2Cl2 / 1 h / 40 °C
View Scheme
参考文献
Mori, Yoko; Morishima, Naohiko
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 1 p. 236 - 241
反应条件
1: 96 percent / NaOMe / methanol / 16 h / Heating
2: 82 percent / NaH / dimethylformamide / 1.5 h / Ambient temperature
View Scheme
参考文献
Krohn, Karsten; Ekkundi, Vadiraj S.; Doering, Detlev; Jones, Peter
Journal of Carbohydrate Chemistry, 1998 , vol. 17, # 2 p. 153 - 170
反应条件
1.1: borane-THF / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere
1.2: 2 h / Inert atmosphere
2.1: sodium periodate; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate / dichloromethane; water / 4 h / 0 - 20 °C
3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h
3.2: 3 h / 0 °C / Inert atmosphere
View Scheme
参考文献
Hsu, Ching-Yun; Lee, I-Chi; Lico, Larry S.; Uang, Biing-Jiun; Hung, Shang-Cheng
Journal of the Chinese Chemical Society, 2012 , vol. 59, # 3 p. 421 - 425
反应条件
diethylamino-sulfur trifluoride in dichloromethane
a) -10 deg C, 0.5 h, b) RT, 1 h;
参考文献
Mori, Yoko; Morishima, Naohiko
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 1 p. 236 - 241
反应条件
dann in Benzol erwaermen;
参考文献
English; Levy
Journal of the American Chemical Society, 1956 , vol. 78, p. 2846
反应条件
triethylamine in 1,2-dichloro-ethane
6 h;
参考文献
Blake, Alexander J.; Gould, Robert O.; McGhie, Karen E.; Paton, R. Michael; Reed, David; et al.
Carbohydrate Research, 1991 , vol. 216, # 1 p. 461 - 474
反应条件
triethylamine in 1,2-dichloro-ethane
6 h;
参考文献
Blake, Alexander J.; Gould, Robert O.; McGhie, Karen E.; Paton, R. Michael; Reed, David; et al.
Carbohydrate Research, 1991 , vol. 216, # 1 p. 461 - 474
反应条件
triethylamine in 1,2-dichloro-ethane
6 h;
参考文献
Blake, Alexander J.; Gould, Robert O.; McGhie, Karen E.; Paton, R. Michael; Reed, David; et al.
Carbohydrate Research, 1991 , vol. 216, # 1 p. 461 - 474
反应条件
triethylamine in 1,2-dichloro-ethane
6 h;
参考文献
Blake, Alexander J.; Gould, Robert O.; McGhie, Karen E.; Paton, R. Michael; Reed, David; et al.
Carbohydrate Research, 1991 , vol. 216, # 1 p. 461 - 474
