1-硫代-b-D-葡萄糖四乙酸酯合成路线 （共 55 条）
反应条件
palladium diacetate; potassium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=100°C; 1 h; Schlenk techniqueInert atmosphereSealed tube; Reagent/catalyst; Overall yield = 63 percent;
参考文献
Brachet, Etienne; Brion, Jean-Daniel; Messaoudi, Samir; Alami, Mouad
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 2-3 p. 477 - 490
反应条件
pyridine; copper diacetate; 4 A molecular sieve in N,N-dimethyl-formamide Substitution; 4 h; Heating;
参考文献
Herradura, Prudencio S.; Pendola, Kathleen A.; Guy, R. Kiplin
Organic Letters, 2000 , vol. 2, # 14 p. 2019 - 2022
反应条件
palladium diacetate; potassium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=100°C; 1 h; Schlenk techniqueInert atmosphereSealed tube; Reagent/catalyst; Overall yield = 63 percent;
参考文献
Brachet, Etienne; Brion, Jean-Daniel; Messaoudi, Samir; Alami, Mouad
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 2-3 p. 477 - 490
反应条件
sodium methylate in methanol 0.25 h; Ambient temperature;
参考文献
Ding, Yili; Contour-Galcera, Marie-Odile; Ebel, Juergen; Ortiz-Mellet, Carmen; Defaye, Jacques
European Journal of Organic Chemistry, 1999 , # 5 p. 1143 - 1152
反应条件
pyridine; copper diacetate; 4 A molecular sieve in N,N-dimethyl-formamide Substitution; 4 h; Heating;
参考文献
Herradura, Prudencio S.; Pendola, Kathleen A.; Guy, R. Kiplin
Organic Letters, 2000 , vol. 2, # 14 p. 2019 - 2022
反应条件
palladium diacetate; potassium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=100°C; 1 h; Schlenk techniqueInert atmosphereSealed tube; Reagent/catalyst; Overall yield = 63 percent;
参考文献
Brachet, Etienne; Brion, Jean-Daniel; Messaoudi, Samir; Alami, Mouad
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 2-3 p. 477 - 490
反应条件
triethylamine in dichloromethane 0.166667 h; Ambient temperature;
参考文献
Fuegedi, Peter; Birberg, Winnie; Garegg, Per J.; Pilotti, Ake
Carbohydrate Research, 1987 , vol. 164, p. 297 - 312
参考文献
Wrede
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1922 , vol. 119, p. 46,56
参考文献
Wrede
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1922 , vol. 119, p. 46,56
Full Text Show Details
Schneider; Bansa
Chemische Berichte, 1931 , vol. 64, p. 1321,1324
反应条件
1: 77 percent / triethylamine / CH2Cl2 / 0.17 h / Ambient temperature 2: sodium methoxide / methanol / Ambient temperature View Scheme
参考文献
Fuegedi, Peter; Birberg, Winnie; Garegg, Per J.; Pilotti, Ake
Carbohydrate Research, 1987 , vol. 164, p. 297 - 312
