2-氟-N-甲氧基-N-甲基苯甲酰胺合成路线 （共 3 条）
反应条件
1: O,N-dimethyl-hydroxylamine hydrochloride With triethylamine in dichloromethane T=0°C; 0.166667 h; 2: 2-fluoro-benzoyl chloride in dichloromethane T=0 - 20°C;
参考文献
OXIGENE, INC.; BAYLOR UNIVERSITY; CHAPLIN, David, J.; GADDALE DEVANNA, Kumar, Kishore; PARKER, Erica; PINNEY, Kevin, G.; SONG, Jiangli; TRAWICK, Mary, L.
Patent: WO2013/142038 A2, 2013 ;
Location in patent: Paragraph 0130 ;
反应条件
triethylamine in dichloromethane T=0 - 20°C;
参考文献
Vitae Pharmaceuticals, Inc.; Boehringer Ingelheim International GmbH
Patent: US2010/331320 A1, 2010 ;
Location in patent: Page/Page column 51; 52 ;
反应条件
in tetrahydrofuran
T=-78 - 20°C;
参考文献
Vitae Pharmaceuticals, Inc.; Boehringer Ingelheim International GmbH
Patent: US2010/331320 A1, 2010 ;
Location in patent: Page/Page column 51; 52 ;
