199620-14-9合成路线 （共 107 条）
反应条件
bromine in gaseous matrix bromination of Cr(CO)6 over the range 410-412 K by dropping sample intohot react. zone, charged with Br2/Ar;
参考文献
Al-Takhin, Ghassan; Connor, Joseph A.; Skinner, Henry A.; Zafarani-Moattar, Mohamed T.
Journal of Organometallic Chemistry, 1984 , vol. 260, # 2 p. 189 - 198
反应条件
in neat (no solvent, solid phase) Electric Arc; pyrolysis at 300 or 400°C for 30 min in N2 atm. or Ar atm.;
参考文献
Journal of Alloys and Compounds, , vol. 417, # 1-2 p. 214 - 219
反应条件
1: diethyl ether 2: water View Scheme
参考文献
Gmelin Handbook: Cr: Org.Verb., 1.1.2.3.3.1, page 106 - 112
Full Text Show Details
Fischer, E. O.; Maasboel, A.
Patent: DE1214233 , 1964 ;
反应条件
chlorine in neat (no solvent) byproducts: CO, COCl2; at ambient temp.;;
参考文献
Gmelin Handbook: Cr: MVol.B, 177, page 365 - 366
反应条件
in tetrahydrofuran; anhydrous butyl ether dissolution of ligand and Cr(CO)6 in a mixt. of butyl ether and THF, heating at 130°C for 24 h under N2, monitoring by IR; concn. under reduced pressure, addn. of hexane, column chromy., elution with n-hexane/CH2Cl2, column chromy., elution with benzene under N2, elem. anal.;
参考文献
Iki, Hideshi; Kikuchi, Taketoshi; Shinkai, Seiji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 2 p. 205 - 210
参考文献
Gmelin Handbook: Cr: Org.Verb., 1.1.2.1.5.2, page 66 - 70
参考文献
Gmelin Handbook: Cr: Org.Verb., 1.1.2.1.5.2, page 66 - 70
参考文献
Fischer, E. O.; Oefele, K.; Essler, H.; Froehlich, W.; Mortensen, J. P.; Semmlinger, W.
Chemische Berichte, 1958 , vol. 91, p. 2763 - 2772
Full Text Show Details
Gmelin Handbook: Cr: Org.Verb., 1.6.1.2.3, page 249 - 253
Full Text Show Details
Mortensen, J. P.
Diss. Muenchen T. H. 1960
Full Text Show Details
Whiting, M. C.
Patent: US3381023 , 1968 ;
反应条件
Bis-(1,3-dihydro-1,3-dimethyl-2H-imidazol-2-ylidene)diiodopalladium; potassium carbonate T=80°C; Suzuki Coupling; 24 h; Inert atmosphere;
参考文献
Lee, Do-Hun; Hahn, Jung-Tai; Jung, Dai-Il
Asian Journal of Chemistry, 2013 , vol. 25, # 15 p. 8611 - 8613
反应条件
in tetrahydrofuran thermal reaction;
参考文献
Fowles, G. W. A.; Jenkins, D. K.
Inorganic Chemistry, 1964 , vol. 3, p. 257 - 259
