2,4,4,6-四氯-2,5-环己二烯-1-酮合成路线 (共 17 条)
反应条件
unter HCl-Entwicklung;
参考文献
Benedikt
Monatshefte fuer Chemie, 1883 , vol. 4, p. 227
反应条件
1.1: dimethylformamide / 0.33 h 1.2: dimethylformamide 2.1: concentrated HCl / methanol; H2O / 0.5 h 3.1: 70 percent / sodium borohydride / aq. ethanol / 0.17 h 4.1: hydrogen / 30percent Pd/C / methanol / 3.5 h 5.1: CrO3; acetic acid / H2O / 0.33 h / 0 - 10 °C View Scheme
参考文献
Heasley, Victor L.; Anderson, James D.; Bowman, Zachery S.; Hanley Jr., John C.; Sigmund, Geoffery A.; Van Horn, David; Shellhamer, Dale F.
Journal of Organic Chemistry, 2002 , vol. 67, # 19 p. 6827 - 6830
反应条件
unter HCl-Entwicklung;
参考文献
Monatshefte fuer Chemie, , vol. 4, p. 227
反应条件
hydrogenchloride; chlorine in acetic acid
T=55 - 70°C; 30 h;
参考文献
Wilson, Gerald J.
Australian Journal of Chemistry, 1987 , vol. 40, # 10 p. 1695 - 1704
反应条件
hydrogenchloride; chlorine
参考文献
Benedikt
Monatshefte fuer Chemie, 1883 , vol. 4, p. 227
反应条件
sulfuric acid; water; chlorine
参考文献
Datta; Mitter
Journal of the American Chemical Society, 1919 , vol. 41, p. 2034
反应条件
sulfuric acid; water; chlorine
参考文献
Datta; Mitter
Journal of the American Chemical Society, 1919 , vol. 41, p. 2034
反应条件
chlorine in acetic acid
Ambient temperature;
参考文献
Dowd, Christopher D.; Paul, D. Brenton
Australian Journal of Chemistry, 1984 , vol. 37, # 1 p. 73 - 86
反应条件
1: chlorine / acetic acid / Ambient temperature
2: chlorine / acetic acid / Ambient temperature
View Scheme
参考文献
Dowd, Christopher D.; Paul, D. Brenton
Australian Journal of Chemistry, 1984 , vol. 37, # 1 p. 73 - 86
反应条件
chlorine; acetic acid
T=15°C;
参考文献
King; Mc Combie
Journal of the Chemical Society, 1913 , vol. 103, p. 230