1-叠氮-1-脱氧-β-D-吡喃葡萄糖苷合成路线 （共 21 条）
反应条件
sodium methylate in methanol; ethylene glycol dimethyl ether T=15°C; 1.5 h;
参考文献
Agricultural and Biological Chemistry, , vol. 47, # 2 p. 281 - 285
反应条件
sodium azide; DMEG; triethylamine in water-d2 T=0°C; 1 h; stereoselective reaction;
参考文献
Chemical Communications, , # 23 p. 3378 - 3379
反应条件
sodium methylate in methanol T=20°C; 18 h;
参考文献
Agricultural and Biological Chemistry, , vol. 47, # 2 p. 281 - 285
反应条件
sodium azide; carbon tetrabromide; triphenylphosphine in N,N-dimethyl-formamide T=20°C; 71 h;
参考文献
Organic Letters, , vol. 12, # 21 p. 4988 - 4991
反应条件
sodium azide; carbon tetrabromide; triphenylphosphine in N,N-dimethyl-formamide T=20°C; 60 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 24 p. 9032 - 9045
反应条件
in water; acetonitrile
反应条件
N-chloro-succinimide; lithium azide; triphenylphosphine in N,N-dimethyl-formamide T=5°C; 22 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 35, # 14 p. 2175 - 2178
反应条件
Yield given. Multistep reaction;
参考文献
Carbohydrate Research, , vol. 117, p. 89 - 94
反应条件
hydrogen azide; di-isopropyl azodicarboxylate; triphenylphosphine in N,N-dimethyl-formamide; toluene T=0 - 20°C; Mitsunobu reaction; 25 h; Inert atmosphere; optical yield given as percent deregioselective reaction;
参考文献
Tetrahedron Letters, , vol. 50, # 50 p. 7043 - 7047
