1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十七氟-10-碘庚烷合成路线 （共 87 条）
2043-53-01,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十七氟-10-碘庚烷
→
反应条件
sodium bromide in water T=100°C; 120 h;
参考文献
Consorti, Crestina S.; Jurisch, Markus; Gladysz, John A.
Organic Letters, 2007 , vol. 9, # 12 p. 2309 - 2312
2043-53-01,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十七氟-10-碘庚烷+
→
反应条件
4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757578 A1, 2007 ;
Location in patent: Page/Page column 6-7; 8-9 ;
2043-53-01,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十七氟-10-碘庚烷
→
反应条件
potassium hydroxide in methanol 6 h; Heating;
参考文献
Ameduri, B.; Boutevin, B.; Nouiri, M.; Talbi, M.
Journal of Fluorine Chemistry, 1995 , vol. 74, # 2 p. 191 - 198
2043-53-01,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十七氟-10-碘庚烷+
→
反应条件
1: malonic acid dimethyl ester With sodium hydride in tetrahydrofuran T=20°C; 0.333333 h; 2: 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-1-iododecane in tetrahydrofuran 18 h; Heating;
参考文献
Trabelsi; Szoenyi; Geribaldi
Journal of Fluorine Chemistry, 2001 , vol. 107, # 1 p. 177 - 181
2043-53-01,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十七氟-10-碘庚烷+
→
反应条件
1: diethyl malonate With sodium hydride in tetrahydrofuran T=20°C; 0.333333 h; 2: 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-1-iododecane in tetrahydrofuran 18 h; Heating;
参考文献
Trabelsi; Szoenyi; Geribaldi
Journal of Fluorine Chemistry, 2001 , vol. 107, # 1 p. 177 - 181
2043-53-01,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十七氟-10-碘庚烷+
→
反应条件
silver(l) oxide T=80°C; 1 h;
参考文献
US2007/123731 A1, ;
Page/Page column 3-4 ;
2043-53-01,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十七氟-10-碘庚烷
→
反应条件
silver(l) oxide T=100°C; 4 h;
参考文献
US2007/123731 A1, ;
Page/Page column 5 ;
2043-53-01,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十七氟-10-碘庚烷+
→
反应条件
silver(l) oxide T=100°C; 4 h;
参考文献
US2007/123731 A1, ;
Page/Page column 5 ;
2043-53-01,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十七氟-10-碘庚烷+
→
反应条件
4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757578 A1, 2007 ;
Location in patent: Page/Page column 8-9 ;
2043-53-01,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十七氟-10-碘庚烷+
→
17741-60-53,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-二十一氟十二烷醇丙烯酸酯
反应条件
4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757578 A1, 2007 ;
Location in patent: Page/Page column 7-8 ;
