N,N-二甲基乙酰基乙酰胺合成路线 （共 24 条）
反应条件
1: KOtBu 2: H2O View Scheme
参考文献
Helvetica Chimica Acta, , vol. 52, p. 2641 - 2657
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 2565 - 2568
反应条件
(i) THF, (ii) aq. MeOH; Multistep reaction;
参考文献
Chemische Berichte, , vol. 112, p. 654 - 662
参考文献
Chemische Berichte, , vol. 92, p. 1456,1458
参考文献
Chemische Berichte, , vol. 92, p. 1456,1458
反应条件
potassium hydroxide; Katamin AB T=100°C; 40 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, p. 1423 - 1426
Zhurnal Organicheskoi Khimii, , vol. 18, # 8 p. 1628 - 1632
参考文献
Shell Devel. Co.
Patent: US2802855 , 1953 ;
反应条件
sodium hydride in tetrahydrofuran
T=0 - 20°C;
参考文献
Nakano, Takeo; Endo, Kohei; Ukaji, Yutaka
Organic Letters, 2014 , vol. 16, # 5 p. 1418 - 1421
反应条件
1: diiodomethane With diethylzinc in hexane; dichloromethane
T=0°C; 0.166667 h;
2: acetoacetic acid dimethylamide in hexane; dichloromethane
T=0°C; 0.25 h;
参考文献
Hilgenkamp, Ramona; Zercher, Charles K
Tetrahedron, 2001 , vol. 57, # 42 p. 8793 - 8800
反应条件
4 A molecular sieve in hexane
T=50°C; 6 h;
参考文献
Nakamura, Masaharu; Fujimoto, Taisuke; Endo, Kohei; Nakamura, Eiichi
Organic Letters, 2004 , vol. 6, # 26 p. 4837 - 4840
