3-苯基-1-对甲苯丙酮合成路线 （共 47 条）
反应条件
1: sodium-compound of cyanoacetic acid amide; ethanol 2: aqueous sulfuric acid View Scheme
参考文献
Barat
Journal of the Indian Chemical Society, 1930 , vol. 7, p. 851,859
反应条件
in tetrahydrofuran T=125°C; 24 h; Sealed tube;
参考文献
Journal of Organic Chemistry, , vol. 76, # 18 p. 7482 - 7490
反应条件
in tetrahydrofuran T=110°C; 12 h; Sealed tube;
参考文献
Journal of Organic Chemistry, , vol. 76, # 18 p. 7482 - 7490
反应条件
in tetrahydrofuran T=125°C; 24 h; Sealed tube;
参考文献
Journal of Organic Chemistry, , vol. 76, # 18 p. 7482 - 7490
反应条件
in tetrahydrofuran T=110°C; 12 h; Sealed tube;
参考文献
Journal of Organic Chemistry, , vol. 76, # 18 p. 7482 - 7490
反应条件
sodium ethanolate in benzene 1 h; Heating;
参考文献
Sabri, Salim S.; Hussein, Ahmad Q.; Al-Hajjar, Farouk H.
Journal of Chemical & Engineering Data, 1985 , vol. 30, # 4 p. 512 - 514
反应条件
triethylamine; palladium on activated charcoal in toluene
T=130°C; Sonogashira coupling; P=15001.5 Torr; 4 h;
参考文献
Liu, Jianhua; Chen, Jing; Xia, Chungu
Journal of Catalysis, 2008 , vol. 253, # 1 p. 50 - 56
反应条件
copper(l) iodide; sodium lauryl sulfate; potassium carbonate; bis-triphenylphosphine-palladium(II) chloride in water
T=65°C; 4 h;
参考文献
Gupta, Sahaj; Sharma, Sudhir K.; Mandadapu, Anil K.; Gauniyal, Harsh M.; Kundu, Bijoy
Tetrahedron Letters, 2011 , vol. 52, # 33 p. 4288 - 4291
反应条件
1: PhCCX (X = Li or MgBr) With indium(III) chloride in tetrahydrofuran
T=-78 - 20°C;
2: carbon monoxide; 1-(iodo)-4-methylbenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=70°C; P=1900 Torr; 3 h;
参考文献
Pena, Miguel A.; Perez Sestelo, Jose; Sarandeses, Luis A.
Synthesis, 2003 , # 5 p. 780 - 784
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine in toluene
T=100°C; carbonylative Sonogashira coupling reaction; P=7600.51 Torr; 3 h; Autoclave;
参考文献
Park, Ahbyeol; Park, Kyungho; Kim, Yong; Lee, Sunwoo
Organic Letters, 2011 , vol. 13, # 5 p. 944 - 947
