2-(乙酰氧基)乙基硫氰酸酯合成路线 (共 3 条)
反应条件
pyridine in dichloromethane T=5 - 20°C; 6 h;
参考文献
ASTELLAS PHARMA INC.
Patent: WO2006/33446 A1, 2006 ;
Location in patent: Page/Page column 26 ;
WO 2006/033446 A1
参考文献
Fokin,A.V. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1975 , vol. 24, p. 334 - 338
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1975 , vol. 24, p. 406 - 410
反应条件
(i) Cl2, (ii) /BRN= 1730731/, 2,6-di-tert-butyl-4-methyl-phenol; Multistep reaction;
参考文献
Guy,R.G.; Pearson,I.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1973 , p. 281 - 284